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HomeMy WebLinkAbout2014-05 Nantucket Landfill - Semi-Annual Environmental Monitoring Report Appendix A Site Plan Appendix B Sampling Results Summary Tables Table 1Nantucket LandfillNantucket, MassachusettsGroundwater Sampling Summary - May 2014Water LevelsMonitoring Well NumberSample Date Ground ElevationTop of PVC ElevationWell Depth (feet)PC2Depth to Groundwater1 (feet)Elevation of Groundwater (feet)MW-1D 5/28/2014 21.06 23.21 75.96 2.47 18.41 4.80MW-1S 5/28/2014 20.71 22.84 26.52 2.46 18.61 4.23MW-3D 5/29/2014 5.53 7.66 71.93 2.37 4.83 2.83MW-3S 5/29/2014 5.35 7.39 12.89 2.63 4.86 2.53MW-4DNM 4NA 5.36 NA NA NM NAMW-4SNM 4NA 4.61 NA NA NM NAMW-5D 5/28/2014 7.38 9.79 62.27 2.41 7.95 1.84MW-5S 5/28/2014 7.82 10.36 13.73 2.75 7.91 2.45MW-6D 5/28/2014 8.26 11.10 62.36 2.78 7.71 3.39MW-6S 5/28/2014 9.03 10.54 14.74 1.63 7.08 3.46MW-7D 5/29/2014 6.79 7.59 60.83 0.76 4.87 2.72MW-7S 5/29/2014 6.70 7.45 15.04 1.02 5.39 2.06MW-8D 5/29/2014 NM 7.36 42.22 1.75 3.48 3.88MW-8S 5/29/2014 NM 6.55 15.32 2.54 2.83 3.72Notes:(1) Depth to water measured from top of PVC(2) PC = Height of protective casing measured from the ground surface(3) PVC Difference = Measured distance between the top of the PVC and the top of the protective casing(4) MW-4S and MW-4D have been buried in fill material and are no longer accessible for samplingNM = Not MeasuredTOC = Top of CasingNA = Not Available Table 2Nantucket LandfillNantucket, MassachusettsGroundwater Sampling Summary - May 2014Metals, Field Parameters, and Indicator ParametersMW-1D MW-1S MW-3D MW-3S MW-5D DUP-1 MW-5S MW-6D MW-6S MW-7D MW-7S MW-8D MW-8SL1411517-02 L1411517-01 L1411620-04 L1411620-03 L1411517-04 L1411517-07 L1411517-03 L1411517-06 L1411517-05 L1411620-06 L1411620-05 L1411620-02 L1411620-015/28/2014 5/28/2014 5/29/2014 5/29/2014 5/28/2014 5/28/2014 5/28/2014 5/28/2014 5/28/2014 5/29/2014 5/29/2014 5/29/2014 5/29/2014Drinking Water StandardsUnitsField ParametersTemperatureNL ºC 10.57 9.53 12.57 10.64 12.39 - 10.80 11.76 10.55 13.28 12.28 11.23 10.52Specific Conductivity NL us/cmc 144 108 650 905 335 - 131 127 1,337 392 1,733 102 447Dissolved Oxygen NL mg/l 6.35 6.53 1.86 1.03 1.90 - 3.35 3.78 3.54 1.44 0.40 6.86 1.04pH6.5-8.4 (3,5) std units 7.01 6.40 6.69 6.69 6.60 - 6.39 6.33 6.30 6.59 6.74 6.62 6.83Indicator ParametersAlkalinityNL mg/l 44.7 3.40 188 326 24.2 24.5 5.60 7.30 9.20 71.9 606 6.60 125TDS (Tot. Dissolved Solids) 500 (3,5) mg/l 99 70 390 580 180 180 82 89 890 220 1,000 46 250Nitrate-Nitrogen 10 (2,4) mg/l 0.247 <0.100 <0.100 <0.100 <0.100 <0.100 0.143 0.892 2.42 <0.100 <0.100 0.747 0.372Cyanide, Total0.2(4) mg/l <0.005 <0.005 <0.005 <0.005 <0.007 <0.005 <0.005 <0.005 0.005 <0.005 0.030 <0.005 <0.005Sulfate250(3,5) mg/l <10 <10 64 11 19 19 <10 <10 16 59 250 <10 <10Chloride250(3,5) mg/l 17 30 67 120 74 76 30 28 430 41 92 21 47COD (Chemical Oxygen Demand ) NL mg/l <20 <20 27 110 <20 <20 <20 <20 25 <20 150 <20 68Dissolved MetalsArsenic10 (2,4) ug/l <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 36.0 <5.0 <5.0Barium2,000 (2,4) ug/l <10.0 <10.0 20.5 50.2 <10.0 <10.0 21.1 <10.0 388 10.7 55 <10.0 17.5Cadmium5 (2,4) ug/l <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0CalciumNL ug/l 14,000 1,700 40,000 69,000 5,300 5,300 1,200 3,100 49,000 20,000 170,000 2,000 24,000Chromium100 (2,4) ug/l <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10Copper1,300 (2,4) ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0Iron300 (3,5) ug/l <50 <50 220 3,300 <50 <50 1,600 <50 120 1,000 59,000 <50 310Lead15 (2,4) ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0Manganese50 (3,5) ug/l <10.0 <10.0 1,140 147 466 466 142 <10.0 158 87.7 1,070 <10.0 110Mercury2 (2,4) ug/l <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20Selenium50 (2,4) ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0Silver100 (3,5) ug/l <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0Sodium20,000 (3) ug/l 10,000 14,000 63,000 75,000 52,000 52,000 18,000 16,000 180,000 26,000 82,000 11,000 28,000Zinc5,000 (3,5) ug/l <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 (8) Initial and final readings were collected for field parameters; final readings are presented. Sample LocationLaboratory IDSample Date NL: No LimitNotes: (1) Highlighted Areas: Concentration Equals or Exceeds Massachusetts or EPA Drinking Water Standards or Guidelines (2) Massachusetts Drinking Water Standard or Maximum Contaminant Level (MCL); Version Spring 2014. (3) Massachusetts Drinking Water Guideline Or Secondary Maximum Contaminant Level (SMCL); Version Spring 2014. (4) EPA Primary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm (5) EPA Secondary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm (6) DUP-1 taken at MW-5D <#.# Not detected to the limit indicated (7) Samples could not be taken from wells MW-4S and MW-4D as they have been filled over. Table 4 Nantucket Landfill Nantucket, Massachusetts Surface Water Sampling Summary - May 2014 Metals, Field Parameters, Indicator Parameters SW-1 SW-2 SW-3 L1411620-07 NS NS 5/29/2014 NS NS NRWQC2,3 Units Field Parameters Temperature NL ºC 16.97 NS NS Specific Conductivity NL us/cmc 39,806 NS NS Dissolved Oxygen NL mg/L 6.20 NS NS pH 6.5-9 standard units 6.87 NS NS Indicator Parameters Alkalinity 20 mg/L 66.3 NS NS TDS (Total Dissolved Solids) NL mg/L 20,000 NS NS Nitrate-Nitrogen NL mg/L <0.100 NS NS Cyanide, Total 0.0052 mg/L <0.005 NS NS Sulfate NL mg/L 1,600 NS NS Chloride 230 mg/L 10,000 NS NS COD (Chemical Oxygen Demand) NL mg/L 1000 NS NS Measured Hardness NL mg/L 2,400 NS NS Dissolved Metals Arsenic 150 ug/L <5.0 NS NS Barium NL ug/L 14.9 NS NS Cadmium 2.214,5 ug/L <0.20 NS NS Calcium NL ug/L 240,000 NS NS Chromium 74 6 ug/L <10 NS NS Copper 135.44,5 ug/L 1.01 NS NS Iron 1,000 ug/L <50 NS NS Lead 59.64,5 ug/L <2.50 NS NS Manganese NL ug/L 115 NS NS Mercury 0.77 ug/L <0.20 NS NS Selenium 5 ug/L <10.0 NS NS Silver 7614,5 ug/L <4.00 NS NS Sodium NL ug/L 6,800,000 NS NS Zinc 1,7454,5 ug/L <50.0 NS NS Notes: (1) Highlighted Areas: Concentration Equals or Exceeds NRWQC (2) NRWQC: National Recommended Water Quality Criteria for Freshwater Based Surface Water, Version 2009 Maximum Concentrations (CMC) values are used Appendix B of the NRWQC Guidance Document (5) See Table 4A for the individual hardness dependent criteria for each sampling location Chromium results represent total chromium, however total chromium is generally assumed to be representative of chromium III, therefore the total chromium results are compared to the chromium III NRWQC (7) Initial and final readings were collected for field parameters; final readings are presented. (8) SW-2 and SW-3 not sampled due to dry conditions. <#.# Not detected to the limit indicated NL: No Limit NS: Not Sampled (6) The NRWQC has established hardness dependent criteria for chromium III and chromium IV. (4) This NRWQC is hardness dependent and is calculated based upon the equations and factors presented in (3) Criterion continuous conentrations (CCC) values are compared to unless none are available, Criterion Sample Location Laboratory ID Sample Date Table 4ANantucket LandfillNantucket, MassachusettsSurface Water Sampling Summary - May 2014Calculated NRWQC for Hardness Dependent MetalsSurface Water Sampling LocationsMeasured Hardness (mg/L)May 2014Cadmium Value (ug/L)Calculated Cadmium Criteria (ug/L)May 2014 Copper Value (ug/L)Calculated Copper Criteria (ug/L)May 2014 Lead Value (ug/L)Calculated Lead Criteria (ug/L)May 2014 Silver Value (ug/L)Calculated Silver Criteria (ug/L)May 2014 Zinc Value (ug/L)Calculated Zinc Criteria (ug/L)SW-12,400<0.202.211.01135.4<2.5059.6<4.00761<50.01,745SW-2NSNSNSNSNSNSNSNSNSNSNSSW-3NSNSNSNSNSNSNSNSNSNSNSNotes:<#.# Not detected to the limit indicated (1) Hardness dependent metals require the NRWQC to be calculated if the sample hardness differs from 100 mg/L. Criteria are calcuated according to the equations and factors presented in Appendix B of the NRWQC Guidance Document dated 2009. (2) Highlighted areas: Concentration equals or exceeds calculated hardness dependent NRWQC. Table 5 Nantucket Landfill Nantucket, Massachusetts Surface Water Sampling Summary - May 2014 Volatile Organic Compounds SW-1 SW-2 SW-3 L1411620-07 NS NS 5/29/2014 NS NS NRWQC2,3 Units Volatile Organic Compounds 1,1,1,2-Tetrachloroethane NL ug/L <0.5 NS NS 1,1,1-Trichloroethane NL ug/L <0.5 NS NS 1,1,2,2-Tetrachloroethane NL ug/L <0.5 NS NS 1,1,2-Trichloroethane NL ug/L <0.75 NS NS 1,1-Dichloroethane NL ug/L <0.75 NS NS 1,1-Dichloroethene NL ug/L <0.5 NS NS 1,1-Dichloropropene NL ug/L <2.5 NS NS 1,2,3- Trichlorobenzene NL ug/L <2.5 NS NS 1,2,3-Trichloropropane NL ug/L <5 NS NS 1,2,4-Trichlorobenzene NL ug/L <2.5 NS NS 1,2,4-Trimethylbenzene NL ug/L <2.5 NS NS 1,2- Dibromo-3-Chloropropane NL ug/L <2.5 NS NS 1,2-Dibromoethane NL ug/L <2 NS NS 1,2-Dichlorobenzene NL ug/L <2.5 NS NS 1,2-Dichloroethane NL ug/L <0.5 NS NS 1,2-Dichloropropane NL ug/L <1.8 NS NS 1,3,5-Trimethylbenzene NL ug/L <2.5 NS NS 1,3-Dichlorobenzene NL ug/L <2.5 NS NS 1,3-Dichloropropane NL ug/L <2.5 NS NS 1,4-Dichlorobenzene NL ug/L <2.5 NS NS 1,4-Dichlorobutane NL ug/L <5 NS NS 1,4-Dioxane NL ug/L <0.147 NS NS 2,2-Dichloropropane NL ug/L <2.5 NS NS 2-Butanone NL ug/L <5 NS NS 2-Chlorotoluene NL ug/L <2.5 NS NS 2-Hexanone NL ug/L <5 NS NS 4-Chlorotoluene NL ug/L <2.5 NS NS 4-Methyl-2-Pentanone NL ug/L <5 NS NS Acetone NL ug/L <5 NS NS Acrylonitrile NL ug/L <5 NS NS Benzene NL ug/L <0.5 NS NS Bromobenzene NL ug/L <2.5 NS NS Bromochloromethane NL ug/L <2.5 NS NS Bromodichloromethane NL ug/L <0.5 NS NS Bromoform NL ug/L <2 NS NS Bromomethane NL ug/L <1 NS NS Carbon Disulfide NL ug/L <5 NS NS Carbon Tetrachloride NL ug/L <0.5 NS NS Chlorobenzene NL ug/L <0.5 NS NS Chloroethane NL ug/L <1 NS NS Chloroform NL ug/L <0.75 NS NS Chloromethane NL ug/L <2.5 NS NS cis 1,2-Dichloroethene NL ug/L <0.5 NS NS cis 1,3-Dichloropropene NL ug/L <0.5 NS NS Dibromochloromethane NL ug/L <0.5 NS NS Dibromomethane NL ug/L <5 NS NS Dichlorodifluoromethane NL ug/L <5 NS NS Ethylbenzene NL ug/L <0.5 NS NS Ethyl Ether NL ug/L <2.5 NS NS Ethyl Methacrylate NL ug/L <5 NS NS Hexachlorobutadiene NL ug/L <0.5 NS NS Isopropylbenzene NL ug/L <0.5 NS NS p-Isopropyltoluene NL ug/L <0.5 NS NS m- and p- Xylenes NL ug/L <1 NS NS Methyl Tert-Butyl Ether NL ug/L <1 NS NS Methylene Chloride NL ug/L <3 NS NS n-Butylbenzene NL ug/L <0.5 NS NS n-Propylbenzene NL ug/L <0.5 NS NS Naphthalene NL ug/L <2.5 NS NS o-Xylene NL ug/L <1 NS NS sec-Butylbenzene NL ug/L <0.5 NS NS Styrene NL ug/L <1 NS NS tert-Butylbenzene NL ug/L <2.5 NS NS Tetrachloroethene NL ug/L <0.5 NS NS Tetrahydrofuran NL ug/L <5 NS NS Toluene NL ug/L <0.75 NS NS trans-1,2-Dichloroethene NL ug/L <0.75 NS NS trans-1,3-Dichloropropene NL ug/L <0.5 NS NS trans-1,4-Dichloro-2-butene NL ug/L <2.5 NS NS Trichloroethene NL ug/L <0.5 NS NS Trichlorofluoromethane NL ug/L <2.5 NS NS Vinyl acetate NL ug/L <5 NS NS Vinyl Chloride NL ug/L <1 NS NS Notes: (1) Highlighted Areas: Concentration Equals or Exceeds NRWQC (2) NRWQC: National Recommended Water Quality Criteria for Freshwater Based Surface Water, Version 2009 (3) Criterion continuous concentrations (CCC) values are compared to unless none are available, Criterion Maximum Concentrations (CMC) values are used <#.# Not detected to the limit indicated NL: No Limit NS:Not Sampled Sample Location Laboratory ID Sample Date Table 6 Nantucket LandfillNantucket, MassachusettsLandfill Gas Sampling Summary - May 2014 LEL (%)Initial Final Initial Final Initial Final Initial Final Initial Final Initial FinalLGW-1 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 1.0 1.0 20.2 20.1 30.10LGW-2 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.5 0.9 20.5 20.2 30.10LGW-3 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 1.1 1.1 19.6 19.6 30.10LGW-4 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.5 0.5 20.2 20.2 30.10LGW-5 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 3.6 3.7 17.1 17.2 30.10LGW-6 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 8.9 9.4 10.4 9.8 30.03LGW-7 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 2.1 2.1 19.4 19.3 30.03LGW-8 Well 5/30/2014 10.0 0.0 0.0 0.0 0.0 0.0 0 0 0.2 0.2 20.0 19.7 30.03LGW-9 Well 5/30/2014 0.0 0.0 0.0 0.0 9.4 13.4 188 268 7.0 10.8 14.6 11.5 30.00Probe-1 Probe 5/30/2014 0.0 0.0 0.0 0.0 10.3 10.3 206 206 17.7 17.7 1.6 1.6 30.00Probe-2 Probe 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 2.4 2.4 17.9 17.9 30.00Probe-3 Probe 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.4 0.4 19.8 20.1 30.00LGW-10 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.8 0.8 20.2 20.3 30.10LGW-11 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.4 0.2 20.5 20.6 30.10LGW-12 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 1.1 1.1 20.1 20.1 30.10LGW-13 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.3 0.2 20.6 20.7 30.03LGW-14 Well 5/30/2014 0.0 0.0 0.0 0.0 11.4 11.6 228 232 23.9 24.4 1.7 1.4 29.98LGW-15 Well 5/30/2014 0.0 0.0 0.0 0.0 35.7 35.9 714 718 26.9 27.4 2.0 1.7 29.98LGW-16 Well 5/30/2014 0.0 0.0 5.5 18.1 35.5 35.6 662 712 33.1 33.3 0.3 0.2 29.98LGW-17 Well 5/30/2014 0.0 0.0 0.0 0.0 33.7 34.0 674 680 24.8 25.2 4.5 4.2 29.98LGW-18 Well 5/30/2014 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 1.7 1.6 19.3 19.3 29.98Notes: (1) Probes and wells were purged for approximately 10 minutes before final readings were recorded. (2) Methane, oxygen and carbon dioxide, measured with GEM-2000 combustible gas meter. (3) Volatile Organic Compounds (VOCs) measured with an Organic Vapor Meter (OVM), lamp eV 10.6. (4) Hydrogen Sulfide measured with an Interscan1000 meter. NS= Not Sampled Gas Monitoring LocationsH2S (ppm) CH4 (% by Vol.) CO2 (%)Barometric Pressure (In. Hg)O2 (%)VOCs (ppmv)Type Date Appendix C Laboratory Reports and Chains of Custody L1411517 CDM Smith, Inc. 1910-97168-CG.SAMP NANTUCKET LF Client: Project Name: Project Number: 06/12/14 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:06121419:26 Page 1 of 88 L1411517-01 L1411517-02 L1411517-03 L1411517-04 L1411517-05 L1411517-06 L1411517-07 L1411517-08 L1411517-09 Alpha Sample ID MW-1S MW-1D MW-5S MW-5D MW-6S MW-6D DUP-1 FB-1 TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411517 06/12/14 05/28/14 13:50 05/28/14 14:40 05/28/14 10:00 05/28/14 10:30 05/28/14 11:45 05/28/14 12:30 05/28/14 00:00 05/28/14 11:00 05/28/14 00:00 Collection Date/Time Serial_No:06121419:26 Page 2 of 88 NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411517 06/12/14 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Serial_No:06121419:26 Page 3 of 88 Case Narrative (continued) NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411517 06/12/14 Sample Receipt L1411517-01 through -08 were field filtered for Dissolved Metals. Cyanide, Total L1411517-04 has an elevated detection limit due to limited sample volume available for analysis. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 06/12/14 Serial_No:06121419:26 Page 4 of 88 ORGANICS Serial_No:06121419:26 Page 5 of 88 VOLATILES Serial_No:06121419:26 Page 6 of 88 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 11:04 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 7 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 8 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 115 103 92 107 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 9 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 11:39 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 10 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 11 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 104 92 111 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 12 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 12:14 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 13 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 14 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 114 103 91 110 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 15 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 12:49 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 16 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 17 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 115 94 94 105 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 18 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 13:24 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 19 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 20 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 110 95 86 111 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 21 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 13:59 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 22 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 23 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 116 98 86 109 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 24 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 14:34 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 25 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 26 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 117 98 94 108 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 27 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-08Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 15:10 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 28 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 29 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 113 98 95 105 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 30 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/12/14 TRIP BLANKClient ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-09Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 15:45 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 31 of 88 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/12/14 TRIP BLANKClient ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 32 of 88 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 2.5 2.5 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 114 95 95 106 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 TRIP BLANKClient ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- Serial_No:06121419:26 Page 33 of 88 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/12/14 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG695364-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 34 of 88 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/12/14 Analyst:PD 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG695364-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 35 of 88 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/12/14 Analyst:PD p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG695364-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 101 105 92 97 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 36 of 88 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 104 107 111 108 108 105 114 112 110 97 114 106 110 110 102 107 95 107 110 108 112 97 95 101 105 107 98 98 106 106 93 105 102 106 102 98 98 87 91 97 106 107 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 7 12 9 3 1 7 15 6 4 4 8 4 4 8 4 9 9 16 13 2 5 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Serial_No:06121419:26 Page 37 of 88 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 98 47 115 104 99 105 106 108 107 108 101 118 119 111 112 104 106 122 89 92 93 90 47 106 104 88 99 104 102 104 104 94 114 112 98 112 84 90 114 80 72 89 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 9 0 8 0 12 6 2 6 3 4 7 3 6 12 0 21 16 7 11 24 4 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Q Q Serial_No:06121419:26 Page 38 of 88 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 107 111 95 97 98 97 99 95 109 106 115 114 107 110 113 111 115 111 97 111 107 98 99 100 78 95 85 96 79 100 98 100 106 100 100 105 104 105 103 90 102 95 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 9 11 5 22 3 13 3 18 9 8 14 7 7 10 7 7 9 7 7 8 12 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Q Serial_No:06121419:26 Page 39 of 88 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 115 113 111 114 108 118 119 77 106 112 106 97 97 103 96 109 106 68 92 116 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 8 15 13 10 12 8 12 12 14 4 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 104 100 96 105 70-130 70-130 70-130 70-130 102 103 90 100 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 06/12/14 Acceptance Criteria Qual Qual Q Qual Serial_No:06121419:26 Page 40 of 88 SEMIVOLATILES Serial_No:06121419:26 Page 41 of 88 FF 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 142 1,4-Dioxane-d8 25 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-01Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 01:22 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 42 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 139 1,4-Dioxane-d8 24 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-02Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 02:10 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 43 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 139 1,4-Dioxane-d8 26 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-03Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 02:58 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 44 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 142 1,4-Dioxane-d8 25 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-04Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 03:47 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 45 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 153 1,4-Dioxane-d8 23 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-05Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 04:35 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 46 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 144 1,4-Dioxane-d8 30 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-06Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 05:24 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 47 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 142 1,4-Dioxane-d8 28 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-07Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 06:12 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 48 of 88 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 147 1,4-Dioxane-d8 27 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/12/14 FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: NANTUCKET, MASample Location: L1411517-08Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 07:01 CM EPA 3510C Extraction Date:06/02/14 05:38 MDL -- Serial_No:06121419:26 Page 49 of 88 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/02/14 12:21 1,8270D-SIMAnalytical Method: Analytical Date: Extraction Method:EPA 3510C Extraction Date:06/02/14 05:38 06/12/14 Analyst:CM 1,4-Dioxane Parameter Result ND RL 150ng/l UnitsQualifier 1,4 Dioxane by 8270D-SIM - Mansfield Lab for sample(s): 01-08 Batch: WG694106-1 1,4-Dioxane-d8 24 15-110 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- Serial_No:06121419:26 Page 50 of 88 1,4-Dioxane 104 105 40-140 1 30 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits 1,4 Dioxane by 8270D-SIM - Mansfield Lab Associated sample(s): 01-08 Batch: WG694106-2 WG694106-3 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 1,4-Dioxane-d8 28 15-11029 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 06/12/14 Acceptance Criteria Qual Qual Qual Serial_No:06121419:26 Page 51 of 88 METALS Serial_No:06121419:26 Page 52 of 88 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 1.7 ND ND ND ND ND ND ND ND 14. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/11/14 11:15 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 06/05/14 10:33 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 53 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 14. ND ND ND ND ND ND ND ND 10. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/11/14 11:21 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 06/05/14 12:33 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 54 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0211 ND 1.2 ND ND 1.6 ND 0.142 ND ND ND 18. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/11/14 11:22 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 06/05/14 12:45 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 55 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 5.3 ND ND ND ND 0.466 ND ND ND 52. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/11/14 11:24 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 06/05/14 12:49 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 56 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.388 ND 49. ND ND 0.12 ND 0.158 ND ND ND 180 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/11/14 11:26 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 06/05/14 12:53 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 57 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 3.1 ND ND ND ND ND ND ND ND 16. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/11/14 11:28 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 06/05/14 12:57 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 58 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 5.3 ND ND ND ND 0.466 ND ND ND 52. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/11/14 11:29 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 06/05/14 13:00 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 59 of 88 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 SAMPLE RESULTS FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411517-08Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/11/14 11:35 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 06/05/14 13:04 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 60 of 88 FF Parameter Parameter Result Result Dilution Factor Dilution Factor Qualifier Qualifier Units Units RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Date Analyzed Date Analyzed Analytical Method Analytical Method Analyst Analyst Date Prepared Date Prepared 06/12/14 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 0.00020 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/11/14 11:08 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A MG MG MG MG MG MG MG MG MG MG MG MG MG AK 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/10/14 13:58 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG694969-1 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG696615-1 NA EPA 7470A Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06121419:26 Page 61 of 88 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved 102 96 104 94 100 102 98 102 96 109 89 100 97 119 - - - - - - - - - - - - - - 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 70-130 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG694969-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG696615-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Serial_No:06121419:26 Page 62 of 88 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND ND 0.125 1.87 0.0518 11 0.19 0.240 0.97 0.515 0.475 0.128 0.0420 23 0.487 0.00540 104 94 102 93 95 96 97 101 95 107 84 90 97 108 - - - - - - - - - - - - - - - - - - - - - - - - - - - - 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694969-4 QC Sample: L1411517-01 Client ID: MW-1S Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG696615-4 QC Sample: L1411517-01 Client ID: MW-1S 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 0.005 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Serial_No:06121419:26 Page 63 of 88 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND ND ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l NC NC NC 0 NC NC NC NC NC NC NC 0 NC NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694969-3 QC Sample: L1411517-01 Client ID: MW-1S Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG696615-3 QC Sample: L1411517-01 Client ID: MW-1S NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1411517Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 06/12/14 Qual Serial_No:06121419:26 Page 64 of 88 INORGANICS & MISCELLANEOUS Serial_No:06121419:26 Page 65 of 88 FF MW-1SClient ID: 05/28/14 13:50Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 3.40 70. ND 30. ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/03/14 14:31 06/04/14 13:35 05/30/14 03:48 06/09/14 16:15 06/05/14 18:09 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 06/03/14 08:29 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 66 of 88 FF MW-1DClient ID: 05/28/14 14:40Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 44.7 99. ND 17. 0.247 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/03/14 14:32 06/04/14 13:36 05/30/14 03:48 06/09/14 16:15 06/05/14 18:09 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 06/03/14 08:29 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 67 of 88 FF MW-5SClient ID: 05/28/14 10:00Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 5.60 82. ND 30. 0.143 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/03/14 14:35 06/04/14 13:36 05/30/14 03:49 06/09/14 16:15 06/05/14 18:09 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 06/03/14 08:29 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 68 of 88 FF MW-5DClient ID: 05/28/14 10:30Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 24.2 180 ND 74. ND 19. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.007 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/06/14 12:51 06/04/14 13:37 05/30/14 03:50 06/09/14 16:15 06/05/14 18:09 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 06/05/14 09:22 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 69 of 88 FF MW-6SClient ID: 05/28/14 11:45Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 9.20 890 0.005 430 2.42 16. 25. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 10 1 1 1 2.00 10 0.005 10 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/06/14 13:01 06/04/14 14:44 05/30/14 03:52 06/09/14 16:15 06/05/14 18:10 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 06/05/14 09:22 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 70 of 88 FF MW-6DClient ID: 05/28/14 12:30Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 7.30 89. ND 28. 0.892 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/02/14 14:58 06/04/14 14:45 05/30/14 03:53 06/09/14 16:15 06/05/14 18:10 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 71 of 88 FF DUP-1Client ID: 05/28/14 00:00Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 24.5 180 ND 76. ND 19. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/02/14 15:01 06/04/14 13:40 05/30/14 03:54 06/09/14 16:15 06/05/14 18:10 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 72 of 88 FF FB-1Client ID: 05/28/14 11:00Date Collected: 05/29/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411517-08Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand ND ND ND ND ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/04/14 12:30 06/02/14 15:16 06/04/14 13:40 05/30/14 03:55 06/09/14 16:15 06/05/14 18:10 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/09/14 16:15 06/05/14 15:25 06/12/14 MDL NA -- -- -- -- -- -- Serial_No:06121419:26 Page 73 of 88 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 Date Analyzed Analytical Method Analyst Date Prepared 06/12/14 Nitrogen, Nitrate Cyanide, Total Cyanide, Total Alkalinity, Total Solids, Total Dissolved Chloride Cyanide, Total Chemical Oxygen Demand Sulfate ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg CaCO3/L mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 0.100 0.005 0.005 2.00 10 1.0 0.005 20 10 05/30/14 03:43 06/03/14 14:21 06/02/14 14:55 06/02/14 10:07 06/04/14 12:30 06/04/14 13:08 06/06/14 12:38 06/05/14 18:08 06/09/14 16:15 30,4500NO3-F 1,9010C/9012B 1,9010C/9012B 30,2320B 30,2540C 1,9251 1,9010C/9012B 30,5220D 1,9038 DB JO JO AN DW LA JO TL MP - 06/03/14 08:29 05/30/14 19:30 - - - 06/05/14 09:22 06/05/14 15:25 06/09/14 16:15 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG693546-1 General Chemistry - Westborough Lab for sample(s): 01-03 Batch: WG693741-1 General Chemistry - Westborough Lab for sample(s): 06-08 Batch: WG693860-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG694352-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG694921-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG694972-1 General Chemistry - Westborough Lab for sample(s): 04-05 Batch: WG695261-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG695420-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG696272-1 MDL -- -- -- NA -- -- -- -- -- Serial_No:06121419:26 Page 74 of 88 Nitrogen, Nitrate Cyanide, Total Cyanide, Total Alkalinity, Total Solids, Total Dissolved Chloride Cyanide, Total 99 94 95 109 98 103 99 - 96 99 - - - 99 90-110 80-120 80-120 90-110 80-120 90-110 80-120 - 2 4 - - - 0 20 20 10 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG693546-2 General Chemistry - Westborough Lab Associated sample(s): 01-03 Batch: WG693741-2 WG693741-3 General Chemistry - Westborough Lab Associated sample(s): 06-08 Batch: WG693860-2 WG693860-3 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG694352-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG694921-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG694972-2 General Chemistry - Westborough Lab Associated sample(s): 04-05 Batch: WG695261-2 WG695261-3 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Qual Qual Serial_No:06121419:26 Page 75 of 88 Chemical Oxygen Demand Sulfate 101 100 - - 93-106 84-119 - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG695420-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG696272-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Serial_No:06121419:26 Page 76 of 88 Nitrogen, Nitrate Cyanide, Total Cyanide, Total Alkalinity, Total Chloride Cyanide, Total Chemical Oxygen Demand Sulfate ND ND ND 2.70 11 0.005 48 ND 1.81 0.202 0.196 104 32 0.200 280 24 45 101 98 101 105 96 97 120 - 0.198 0.196 - - 0.195 - - - 99 98 - - 94 - - 83-113 80-120 80-120 86-116 58-140 80-120 84-120 55-147 - 2 1 - - 3 - - 17 20 20 10 7 20 12 14 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG693546-4 QC Sample: L1411552-01 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG693741-4 WG693741-5 QC Sample: L1411517-02 Client ID: MW- 1D General Chemistry - Westborough Lab Associated sample(s): 06-08 QC Batch ID: WG693860-4 WG693860-5 QC Sample: L1411620-06 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694352-4 QC Sample: L1411552-09 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694972-4 QC Sample: L1411552-09 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 04-05 QC Batch ID: WG695261-4 WG695261-5 QC Sample: L1411517-05 Client ID: MW- 6S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG695420-3 QC Sample: L1411552-01 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG696272-4 QC Sample: L1411517-01 Client ID: MW-1S 4 0.2 0.2 100 20 0.2 238 20 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411517 06/12/14 Qual Q Qual Qual Serial_No:06121419:26 Page 77 of 88 Nitrogen, Nitrate Alkalinity, Total Solids, Total Dissolved Chloride Chemical Oxygen Demand Sulfate ND 2.70 21000 11 48 ND 0.463 2.90 22000 11 43 ND mg/l mg CaCO3/L mg/l mg/l mg/l mg/l NC 7 5 0 11 NC 17 10 17 7 12 14 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG693546-3 QC Sample: L1411552-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694352-3 QC Sample: L1411552-09 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694921-3 QC Sample: L1411585-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG694972-3 QC Sample: L1411552-09 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG695420-4 QC Sample: L1411552-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG696272-3 QC Sample: L1411517-01 Client ID: MW-1S NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1411517Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 06/12/14 Qual Serial_No:06121419:26 Page 78 of 88 *Values in parentheses indicate holding time in days L1411517-01A L1411517-01B L1411517-01C L1411517-01D L1411517-01E L1411517-01F L1411517-01G L1411517-01H L1411517-01I L1411517-01J L1411517-02A L1411517-02B L1411517-02D L1411517-02E L1411517-02F L1411517-02G Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved C C C C C C C C A A A A A A A A N/A N/A N/A >12 <2 <2 N/A 7 7 7 N/A N/A >12 <2 <2 N/A 4.7 4.7 4.7 4.7 4.7 4.7 4.7 4.7 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A B C Absent Absent Absent Cooler Custody SealCooler Information NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) Project Name: Project Number: L1411517Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/12/14 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:06121419:26 Page 79 of 88 *Values in parentheses indicate holding time in days L1411517-02H L1411517-02I L1411517-02J L1411517-03A L1411517-03B L1411517-03C L1411517-03D L1411517-03E L1411517-03F L1411517-03G L1411517-03H L1411517-03I L1411517-03J L1411517-04A L1411517-04B L1411517-04C L1411517-04D L1411517-04E L1411517-04F L1411517-04G L1411517-04H L1411517-04I L1411517-04J L1411517-05A L1411517-05B L1411517-05C Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved A C C B B B B B B B B B B B B B B B B B B B B A A A 7 7 7 N/A N/A N/A >12 <2 <2 N/A 7 7 7 N/A N/A N/A >12 <2 <2 N/A 7 7 7 N/A N/A N/A 4.2 4.7 4.7 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 4.2 4.2 4.2 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) Project Name: Project Number: L1411517Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/12/14 Serial_No:06121419:26 Page 80 of 88 *Values in parentheses indicate holding time in days L1411517-05D L1411517-05E L1411517-05F L1411517-05G L1411517-05H L1411517-05I L1411517-05J L1411517-06A L1411517-06B L1411517-06C L1411517-06D L1411517-06E L1411517-06F L1411517-06G L1411517-06H L1411517-06I L1411517-06J L1411517-07A L1411517-07B L1411517-07C L1411517-07D L1411517-07E L1411517-07F L1411517-07G Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved A A A A A A A A A A A A A A A A A B B B B B B B >12 <2 <2 N/A 7 7 7 N/A N/A N/A >12 <2 <2 N/A 7 7 7 N/A N/A N/A >12 <2 <2 N/A 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 4.2 2.0 2.0 2.0 2.0 2.0 2.0 2.0 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) Project Name: Project Number: L1411517Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/12/14 Serial_No:06121419:26 Page 81 of 88 *Values in parentheses indicate holding time in days L1411517-07H L1411517-07I L1411517-07J L1411517-08A L1411517-08B L1411517-08C L1411517-08D L1411517-08E L1411517-08F L1411517-08G L1411517-08H L1411517-08I L1411517-08J L1411517-09A Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved B C C C C C C C C C C B B C 7 7 7 N/A N/A N/A >12 <2 <2 N/A 7 7 7 N/A 2.0 4.7 4.7 4.7 4.7 4.7 4.7 4.7 4.7 4.7 4.7 2.0 2.0 4.7 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) Project Name: Project Number: L1411517Lab Number: Report Date: L1411517-04D L1411517-05D Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/12/14 Container Comments Serial_No:06121419:26 Page 82 of 88 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1411517NANTUCKET LF 1910-97168-CG.SAMP 06/12/14 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total' result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082. Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:06121419:26 Page 83 of 88 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1411517NANTUCKET LF 1910-97168-CG.SAMP 06/12/14 Data Qualifiers H I M NJ P Q R RE S - - - - - - - - - The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The lower value for the two columns has been reported due to obvious interference. Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. Analytical results are from modified screening analysis. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:06121419:26 Page 84 of 88 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1411517NANTUCKET LF 1910-97168-CG.SAMP REFERENCES 06/12/14 Serial_No:06121419:26 Page 85 of 88 Certification Information Last revised April 15, 2014 The following analytes are not included in our NELAP Scope of Accreditation: Westborough Facility EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone (MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5-Trichlorobenzene, 4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, Iodomethane (methyl iodide), Methyl methacrylate, Azobenzene. EPA 8330A/B: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline, 4-Methylphenol. SM4500: Soil: Total Phosphorus, TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Mansfield Facility EPA 8270D: Biphenyl. EPA 2540D: TSS EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation, Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B EPA 332: Perchlorate. Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn; EPA 200.7: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn; EPA 245.1, SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2340B, SM2320B, SM4500CL-E, SM4500F-BC, SM426C, SM4500NH3-BH, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, SM4500P-B, E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. EPA 624: Volatile Halocarbons & Aromatics, EPA 608: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9222D-MF. For a complete listing of analytes and methods, please contact your Alpha Project Manager. Serial_No:06121419:26 Page 86 of 88 Serial_No:06121419:26 Page 87 of 88 .,$AMPLE HANDLING ,,~~\'Filtra.tion.,.-_liit"Oor:1e .. o Not needed [J Lab to doPreservation. IJ Lab 10do' (PIe•••spodfy be""") Sample Specific Comments Are MCP Analytical Methods Required? IsMatrix Spike (MS)Required on this SOG?(If yes see note In Comments) Are CT RCP (Reasonable Confidence Protocols)Required? ,boo Time: IJ RUSH {MIy '''Ill!nnodd~ Collection sample Date TIme Matrix Turn.Around Time ~ndard :,- Sample 10 CHAIN OF CUSTODY . .\4-4S'2~~81 ~.1"1 -'($1 .b~ PLEASE ANSWER QUESTIONS ABOVE! Phone: Fax: Email: ALP.HA Quote #:I----':...!..>.~~~:......:..L::..,..=.=.:.»LL---__l. Serial_No:06121419:26 Page 88 of 88 L1411620 CDM Smith, Inc. 1910-97168-CG.SAMP NANTUCKET LF Client: Project Name: Project Number: 06/13/14 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:06131415:12 Page 1 of 86 L1411620-01 L1411620-02 L1411620-03 L1411620-04 L1411620-05 L1411620-06 L1411620-07 L1411620-08 Alpha Sample ID MW-8S MW-8D MW-3S MW-3D MW-7S MW-7D SW-1 TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411620 06/13/14 05/29/14 09:45 05/29/14 10:15 05/29/14 11:30 05/29/14 12:30 05/29/14 13:30 05/29/14 14:00 05/29/14 15:20 05/29/14 00:00 Collection Date/Time Serial_No:06131415:12 Page 2 of 86 NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411620 06/13/14 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Serial_No:06131415:12 Page 3 of 86 Case Narrative (continued) NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1411620 06/13/14 Sample Receipt The samples were field filtered for Dissolved Metals. The samples were received via express courier (Federal Express) in coolers with ice; however, one of the coolers was above the required temperature range. The client was notified of the exceedance, and all requested analyses were performed. L1411620-01 and -05 were received above the appropriate pH for the Dissolved Metals analysis. The laboratory added additional HNO3 to a pH <2. Total Metals The WG694927-4 MS recovery for hardness (1210%) performed on L1411620-07, does not apply because the sample concentration is greater than four times the spike amount added. Dissolved Metals The WG695080-4 MS recoveries for calcium (0%) and sodium (0%), performed on L1411620-07, do not apply because the sample concentrations are greater than four times the spike amounts added. Nitrogen, Nitrate L1411620-01 through -07 were analyzed for Nitrite within the method required holding time. Aliquots of sample were then preserved and analyzed for Nitrate. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 06/13/14 Serial_No:06131415:12 Page 4 of 86 ORGANICS Serial_No:06131415:12 Page 5 of 86 VOLATILES Serial_No:06131415:12 Page 6 of 86 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 16:20 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 7 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND 5.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 8 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 113 97 91 104 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 9 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 16:55 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 10 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 11 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 118 103 91 105 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 12 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 17:30 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 13 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 14 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 115 98 94 109 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 15 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 18:05 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 16 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 17 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 116 97 93 108 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 18 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.56 ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 18:40 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 19 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 20 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 114 99 94 109 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 21 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 19:15 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 22 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 23 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 113 98 92 107 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 24 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 19:50 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 25 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 26 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 120 98 91 108 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- Serial_No:06131415:12 Page 27 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 06/13/14 TRIP BLANKClient ID: 05/29/14 00:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-08Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 06/05/14 20:25 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 28 of 86 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 06/13/14 TRIP BLANKClient ID: 05/29/14 00:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-08Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 29 of 86 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether Parameter Result Dilution Factor ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 2.5 2.5 2.5 2.5 2.5 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 115 100 94 105 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 TRIP BLANKClient ID: 05/29/14 00:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-08Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- Serial_No:06131415:12 Page 30 of 86 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/13/14 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,3-Dichloropropene, Total 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloroethene, Total Trichloroethene 1,2-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 0.50 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG695364-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 31 of 86 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/13/14 Analyst:PD 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 2.5 2.5 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG695364-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 32 of 86 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/05/14 10:28 1,8260CAnalytical Method: Analytical Date: 06/13/14 Analyst:PD p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG695364-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 101 105 92 97 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 33 of 86 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 104 107 111 108 108 105 114 112 110 97 114 106 110 110 102 107 95 107 110 108 112 97 95 101 105 107 98 98 106 106 93 105 102 106 102 98 98 87 91 97 106 107 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 7 12 9 3 1 7 15 6 4 4 8 4 4 8 4 9 9 16 13 2 5 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Serial_No:06131415:12 Page 34 of 86 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 98 47 115 104 99 105 106 108 107 108 101 118 119 111 112 104 106 122 89 92 93 90 47 106 104 88 99 104 102 104 104 94 114 112 98 112 84 90 114 80 72 89 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 9 0 8 0 12 6 2 6 3 4 7 3 6 12 0 21 16 7 11 24 4 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Q Q Serial_No:06131415:12 Page 35 of 86 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 107 111 95 97 98 97 99 95 109 106 115 114 107 110 113 111 115 111 97 111 107 98 99 100 78 95 85 96 79 100 98 100 106 100 100 105 104 105 103 90 102 95 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 9 11 5 22 3 13 3 18 9 8 14 7 7 10 7 7 9 7 7 8 12 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Q Serial_No:06131415:12 Page 36 of 86 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 115 113 111 114 108 118 119 77 106 112 106 97 97 103 96 109 106 68 92 116 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 8 15 13 10 12 8 12 12 14 4 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG695364-1 WG695364-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 104 100 96 105 70-130 70-130 70-130 70-130 102 103 90 100 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 06/13/14 Acceptance Criteria Qual Qual Q Qual Serial_No:06131415:12 Page 37 of 86 SEMIVOLATILES Serial_No:06131415:12 Page 38 of 86 FF 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 144 1,4-Dioxane-d8 23 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-01Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 13:45 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 39 of 86 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 142 1,4-Dioxane-d8 25 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-02Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 14:34 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 40 of 86 1,4-Dioxane Parameter Result Dilution Factor 2080 ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 142 1,4-Dioxane-d8 23 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-03Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 15:22 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 41 of 86 1,4-Dioxane Parameter Result Dilution Factor 1190 ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 144 1,4-Dioxane-d8 25 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-04Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 16:11 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 42 of 86 1,4-Dioxane Parameter Result Dilution Factor 1380 ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 142 1,4-Dioxane-d8 18 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-05Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 17:00 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 43 of 86 1,4-Dioxane Parameter Result Dilution Factor 350 ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 144 1,4-Dioxane-d8 20 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-06Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 17:49 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 44 of 86 1,4-Dioxane Parameter Result Dilution Factor ND ng/l 1 Qualifier Units RL 1,4 Dioxane by 8270D-SIM - Mansfield Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 147 1,4-Dioxane-d8 26 15-110 Acceptance CriteriaSurrogate % Recovery Qualifier 06/13/14 SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: NANTUCKET, MASample Location: L1411620-07Lab ID: Field Prep:See Narrative Matrix:Water Extraction Method: Analytical Method: Analytical Date: Analyst: 1,8270D-SIM 06/03/14 18:37 CM EPA 3510C Extraction Date:06/03/14 05:38 MDL -- Serial_No:06131415:12 Page 45 of 86 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/03/14 11:18 1,8270D-SIMAnalytical Method: Analytical Date: Extraction Method:EPA 3510C Extraction Date:06/03/14 05:38 06/13/14 Analyst:CM 1,4-Dioxane Parameter Result ND RL 150ng/l UnitsQualifier 1,4 Dioxane by 8270D-SIM - Mansfield Lab for sample(s): 01-07 Batch: WG694469-1 1,4-Dioxane-d8 32 15-110 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- Serial_No:06131415:12 Page 46 of 86 1,4-Dioxane 102 104 40-140 2 30 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits 1,4 Dioxane by 8270D-SIM - Mansfield Lab Associated sample(s): 01-07 Batch: WG694469-2 WG694469-3 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 1,4-Dioxane-d8 25 15-11023 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 06/13/14 Acceptance Criteria Qual Qual Qual Serial_No:06131415:12 Page 47 of 86 METALS Serial_No:06131415:12 Page 48 of 86 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0175 ND 24. ND ND 0.31 ND 0.110 ND ND ND 28. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/11/14 14:31 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 06/05/14 13:08 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/11/14 11:49 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 49 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 2.0 ND ND ND ND ND ND ND ND 11. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/11/14 14:37 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 06/05/14 13:12 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/11/14 11:49 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 50 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0502 ND 69. ND ND 3.3 ND 0.147 ND ND ND 75. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/11/14 14:39 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 06/05/14 13:16 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MG MG MG MG MG MG MG MG MG AK MG MG MG MG 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/11/14 11:49 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 51 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0205 ND 40. ND ND 0.22 ND 1.14 ND ND ND 63. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/06/14 13:54 06/11/14 14:40 06/06/14 13:54 06/06/14 13:54 06/07/14 11:13 06/06/14 13:54 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C JH JH JH JH JH JH JH JH JH AK JH JH BC JH 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/11/14 11:49 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 7470A EPA 3005A EPA 3005A EPA 3005A EPA 3005A Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 52 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 0.0360 0.0550 ND 170 ND ND 59. ND 1.07 ND ND ND 82. 0.316 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/06/14 13:57 06/11/14 14:42 06/06/14 13:57 06/06/14 13:57 06/07/14 11:17 06/06/14 13:57 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C JH JH JH JH JH JH JH JH JH AK JH JH BC JH 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/11/14 11:49 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 7470A EPA 3005A EPA 3005A EPA 3005A EPA 3005A Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 53 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0107 ND 20. ND ND 1.0 ND 0.0877 ND ND ND 26. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/06/14 14:01 06/11/14 14:48 06/06/14 14:01 06/06/14 14:01 06/07/14 11:32 06/06/14 14:01 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C JH JH JH JH JH JH JH JH JH AK JH JH BC JH 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/11/14 11:49 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 7470A EPA 3005A EPA 3005A EPA 3005A EPA 3005A Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 54 of 86 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 SAMPLE RESULTS SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: Matrix:Water NANTUCKET, MASample Location: L1411620-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Total Hardness by SM 2340B - Westborough Lab Dissolved Metals - Westborough Lab Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 2400 ND 0.0149 ND 240 ND 0.00101 ND ND 0.115 ND ND ND 6800 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 100 1 0.66 0.0050 0.0100 0.00020 0.10 0.010 0.00100 0.050 0.00250 0.0100 0.00020 0.0100 0.00400 200 0.0500 06/04/14 09:28 06/06/14 12:31 06/06/14 12:31 06/05/14 11:45 06/06/14 12:31 06/06/14 12:31 06/05/14 11:45 06/06/14 12:31 06/05/14 11:45 06/06/14 12:31 06/11/14 14:49 06/06/14 12:31 06/05/14 11:45 06/07/14 10:57 06/06/14 12:31 1,6010C 1,6010C 1,6010C 1,6020A 1,6010C 1,6010C 1,6020A 1,6010C 1,6020A 1,6010C 1,7470A 1,6010C 1,6020A 1,6010C 1,6010C JH JH JH KL JH JH KL JH KL JH AK JH KL BC JH 06/03/14 15:01 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/11/14 11:49 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 3005A EPA 7470A EPA 3005A EPA 3005A EPA 3005A EPA 3005A Prep MethodMDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 55 of 86 FF Parameter Parameter Parameter Result Result Result Dilution Factor Dilution Factor Dilution Factor Qualifier Qualifier Qualifier Units Units Units RL RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Date Analyzed Date Analyzed Date Analyzed Analytical Method Analytical Method Analytical Method Analyst Analyst Analyst Date Prepared Date Prepared Date Prepared 06/13/14 Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.66 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 0.00020 0.00100 0.00100 0.00040 06/04/14 09:21 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 10:48 06/05/14 11:30 06/05/14 11:30 06/05/14 11:30 06/05/14 11:30 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6020A 1,6020A 1,6020A 1,6020A JH MG MG MG MG MG MG MG MG MG MG MG MG MG KL KL KL KL 06/03/14 15:01 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 12:08 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 Total Hardness by SM 2340B - Westborough Lab for sample(s): 07 Batch: WG694927-1 Dissolved Metals - Westborough Lab for sample(s): 01-03 Batch: WG694969-1 Dissolved Metals - Westborough Lab for sample(s): 07 Batch: WG695078-1 EPA 3005A NA Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL MDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 56 of 86 Parameter Parameter Result Result Dilution Factor Dilution Factor Qualifier Qualifier Units Units RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Date Analyzed Date Analyzed Analytical Method Analytical Method Analyst Analyst Date Prepared Date Prepared 06/13/14 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 0.00020 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/06/14 12:00 06/07/14 10:50 06/06/14 12:00 06/11/14 14:28 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A JH JH JH JH JH JH JH JH JH JH JH BC JH AK 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/04/14 16:07 06/11/14 11:49 Dissolved Metals - Westborough Lab for sample(s): 04-07 Batch: WG695080-1 Dissolved Metals - Westborough Lab for sample(s): 01-07 Batch: WG696955-1 EPA 3005A EPA 3005A EPA 7470A Digestion Method: Digestion Method: Digestion Method: Prep Information Prep Information Prep Information MDL MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:06131415:12 Page 57 of 86 Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 97 102 96 104 94 100 102 98 102 96 109 89 100 97 - - - - - - - - - - - - - - 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07 Batch: WG694927-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-03 Batch: WG694969-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Serial_No:06131415:12 Page 58 of 86 Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 112 98 106 97 93 87 98 98 85 88 90 96 92 98 86 110 92 - - - - - - - - - - - - - - - - - 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 07 Batch: WG695078-2 Dissolved Metals - Westborough Lab Associated sample(s): 04-07 Batch: WG695080-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Serial_No:06131415:12 Page 59 of 86 Mercury, Dissolved 113 -70-130 - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-07 Batch: WG696955-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Serial_No:06131415:12 Page 60 of 86 Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved 2400 ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND ND 0.00101 ND ND 3200 0.125 1.87 0.0518 11 0.19 0.240 0.97 0.515 0.475 0.128 0.0420 23 0.487 0.05299 0.2364 0.5617 0.04702 1210 104 94 102 93 95 96 97 101 95 107 84 90 97 104 94 110 94 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07 QC Batch ID: WG694927-4 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG694969-4 QC Sample: L1411517-01 Client ID: MS Sample Dissolved Metals - Westborough Lab Associated sample(s): 07 QC Batch ID: WG695078-4 QC Sample: L1411620-07 Client ID: SW-1 66.2 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 0.051 0.25 0.51 0.05 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Q Qual Qual Serial_No:06131415:12 Page 61 of 86 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved ND 0.0149 ND 240 ND ND ND ND 0.115 ND ND 6800 ND ND 0.148 1.87 0.0484 230 0.18 0.285 0.92 0.428 0.564 0.148 0.0626 6300 0.467 0.00549 123 93 95 0 90 114 92 84 90 123 125 0 93 110 - - - - - - - - - - - - - - - - - - - - - - - - - - - - 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 04-07 QC Batch ID: WG695080-4 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG696955-4 QC Sample: L1411620-01 Client ID: MW-8S 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 0.005 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Q Q Serial_No:06131415:12 Page 62 of 86 Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 2400 ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND 2500 ND ND ND 1.7 ND ND ND ND ND ND ND 14 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 4 NC NC NC 0 NC NC NC NC NC NC NC 0 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07 QC Batch ID: WG694927-3 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG694969-3 QC Sample: L1411517-01 Client ID: DUP Sample NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1411620Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 06/13/14 Qual Serial_No:06131415:12 Page 63 of 86 Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Arsenic, Dissolved Barium, Dissolved Calcium, Dissolved Chromium, Dissolved Iron, Dissolved Manganese, Dissolved Selenium, Dissolved Zinc, Dissolved Sodium, Dissolved Mercury, Dissolved ND 0.00101 ND ND ND 0.0149 240 ND ND 0.115 ND ND 6800 ND ND ND ND ND ND 0.0147 240 ND ND 0.116 ND ND 6500 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l NC NC NC NC NC 1 0 NC NC 1 NC NC 5 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 07 QC Batch ID: WG695078-3 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 04-07 QC Batch ID: WG695080-3 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 04-07 QC Batch ID: WG695080-3 QC Sample: L1411620-07 Client ID: SW-1 Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG696955-3 QC Sample: L1411620-01 Client ID: MW-8S NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1411620Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 06/13/14 Serial_No:06131415:12 Page 64 of 86 INORGANICS & MISCELLANEOUS Serial_No:06131415:12 Page 65 of 86 FF MW-8SClient ID: 05/29/14 09:45Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 125. 250 ND 47. 0.372 ND 68. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:08 06/04/14 14:05 06/03/14 02:47 06/10/14 14:00 06/06/14 18:35 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 66 of 86 FF MW-8DClient ID: 05/29/14 10:15Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 6.60 46. ND 21. 0.747 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:02 06/04/14 14:06 06/03/14 02:49 06/10/14 14:00 06/06/14 18:35 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 67 of 86 FF MW-3SClient ID: 05/29/14 11:30Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 326. 580 ND 120 ND 11. 110 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 5 1 1 1 2.00 10 0.005 5.0 0.100 10 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:39 06/04/14 14:58 06/03/14 02:50 06/10/14 14:00 06/06/14 18:35 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/31/14 10:05 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 68 of 86 FF MW-3DClient ID: 05/29/14 12:30Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 188. 390 ND 67. ND 64. 27. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:18 06/04/14 14:09 06/03/14 02:51 06/10/14 14:00 06/06/14 18:35 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 69 of 86 FF MW-7SClient ID: 05/29/14 13:30Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 606. 1000 0.030 92. ND 250 150 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 2 1 1 1 1 10 1 4.00 10 0.005 1.0 0.100 100 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:06 06/04/14 14:12 06/03/14 02:51 06/10/14 14:00 06/06/14 18:35 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 70 of 86 FF MW-7DClient ID: 05/29/14 14:00Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 71.9 220 ND 41. ND 59. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:07 06/04/14 14:12 06/03/14 02:52 06/10/14 14:00 06/06/14 18:36 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 71 of 86 FF SW-1Client ID: 05/29/14 15:20Date Collected: 05/30/14Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1411620-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 66.3 20000 ND 10000 ND 1600 1000 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 500 1 50 1 2.00 10 0.005 500 0.100 500 20 06/02/14 10:07 06/05/14 12:45 06/02/14 15:08 06/04/14 15:09 06/03/14 02:53 06/10/14 14:00 06/06/14 18:41 30,2320B 30,2540C 1,9010C/9012B 1,9251 30,4500NO3-F 1,9038 30,5220D AN DW JO LA DB MP TL Date Prepared - - 05/30/14 19:30 - - 06/10/14 14:00 06/06/14 15:30 06/13/14 MDL NA -- -- -- -- -- -- Serial_No:06131415:12 Page 72 of 86 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 Date Analyzed Analytical Method Analyst Date Prepared 06/13/14 Cyanide, Total Alkalinity, Total Chloride Nitrogen, Nitrate Solids, Total Dissolved Chemical Oxygen Demand Sulfate ND ND ND ND ND ND ND mg/l mg CaCO3/L mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 0.005 2.00 1.0 0.100 10 20 10 06/02/14 14:55 06/02/14 10:07 06/04/14 14:04 06/03/14 02:03 06/05/14 12:45 06/06/14 18:31 06/10/14 14:00 1,9010C/9012B 30,2320B 1,9251 30,4500NO3-F 30,2540C 30,5220D 1,9038 JO AN LA DB DW TL MP 05/30/14 19:30 - - - - 06/06/14 15:30 06/10/14 14:00 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG693860-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG694353-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG694974-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG695164-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG695256-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG695786-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG696555-1 MDL -- NA -- -- -- -- -- Serial_No:06131415:12 Page 73 of 86 Cyanide, Total Alkalinity, Total Chloride Nitrogen, Nitrate Solids, Total Dissolved Chemical Oxygen Demand Sulfate 95 102 103 99 94 99 105 99 - - - - - - 80-120 90-110 90-110 90-110 80-120 93-106 84-119 4 - - - - - - 20 10 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG693860-2 WG693860-3 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG694353-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG694974-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG695164-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG695256-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG695786-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG696555-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Serial_No:06131415:12 Page 74 of 86 Cyanide, Total Alkalinity, Total Chloride Nitrogen, Nitrate Chemical Oxygen Demand Sulfate ND 90.8 67 0.372 ND 64 0.196 186 84 4.47 240 170 98 95 85 102 101 106 0.196 - - - - - 98 - - - - - 80-120 86-116 58-140 83-113 84-120 55-147 1 - - - - - 20 10 7 17 12 14 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG693860-4 WG693860-5 QC Sample: L1411620-06 Client ID: MW- 7D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG694353-4 QC Sample: L1411150-03 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG694974-4 QC Sample: L1411620-04 Client ID: MW-3D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG695164-4 QC Sample: L1411620-01 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG695786-3 QC Sample: L1411620-02 Client ID: MW-8D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG696555-4 QC Sample: L1411620-04 Client ID: MW-3D 0.2 100 20 4 238 100 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1411620 06/13/14 Qual Qual Qual Serial_No:06131415:12 Page 75 of 86 Alkalinity, Total Chloride Nitrogen, Nitrate Solids, Total Dissolved Chemical Oxygen Demand Sulfate 90.8 67 0.372 490 ND ND 89.6 67 0.368 460 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l 1 0 0 6 NC NC 10 7 17 17 12 14 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG694353-3 QC Sample: L1411150-03 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG694974-3 QC Sample: L1411620-04 Client ID: MW-3D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG695164-3 QC Sample: L1411620-01 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG695256-3 QC Sample: L1411781-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG695786-4 QC Sample: L1411620-02 Client ID: MW-8D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG696555-3 QC Sample: L1411620-02 Client ID: MW-8D NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1411620Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 06/13/14 Qual Serial_No:06131415:12 Page 76 of 86 *Values in parentheses indicate holding time in days L1411620-01A L1411620-01B L1411620-01C L1411620-01D L1411620-01E L1411620-01F L1411620-01G L1411620-01H L1411620-01I L1411620-01J L1411620-02A L1411620-02B L1411620-02C L1411620-02D L1411620-02E L1411620-02F L1411620-02G Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved B B B B B B B B B B C C C C C C C N/A N/A N/A >12 <2 <2 N/A 8 8 8 N/A N/A N/A >12 <2 <2 N/A 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 5.7 5.7 5.7 5.7 5.7 5.7 5.7 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A B C Absent Absent Absent Cooler Custody SealCooler Information NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) Project Name: Project Number: L1411620Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/13/14 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:06131415:12 Page 77 of 86 *Values in parentheses indicate holding time in days L1411620-02H L1411620-02I L1411620-02J L1411620-03A L1411620-03B L1411620-03C L1411620-03D L1411620-03E L1411620-03F L1411620-03G L1411620-03H L1411620-03I L1411620-03J L1411620-04A L1411620-04B L1411620-04C L1411620-04D L1411620-04E L1411620-04F L1411620-04G L1411620-04H L1411620-04I L1411620-04J L1411620-05A L1411620-05B L1411620-05C Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved C C C C C C C C C C C C C C C C C C C C C C C B B B 8 8 8 N/A N/A N/A >12 <2 <2 N/A 8 8 8 N/A N/A N/A >12 <2 <2 N/A 8 8 8 N/A N/A N/A 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 5.7 4.3 4.3 4.3 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) Project Name: Project Number: L1411620Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/13/14 Serial_No:06131415:12 Page 78 of 86 *Values in parentheses indicate holding time in days L1411620-05D L1411620-05E L1411620-05F L1411620-05G L1411620-05H L1411620-05I L1411620-05J L1411620-06A L1411620-06B L1411620-06C L1411620-06D L1411620-06E L1411620-06F L1411620-06G L1411620-06H L1411620-06I L1411620-06J L1411620-07A L1411620-07B L1411620-07C L1411620-07D L1411620-07E L1411620-07F L1411620-07G Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml H2SO4 preserved Plastic 250ml unpreserved Plastic 500ml unpreserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved B B B B B B B B B B B B B B B B B B A A A A A A >12 <2 <2 N/A 8 8 8 N/A N/A N/A >12 <2 <2 N/A 8 8 8 N/A N/A N/A N/A <2 <2 >12 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 4.3 8.9 8.9 8.9 8.9 8.9 8.9 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) COD-5220(28) ALK-T-2320(14) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) CU-6020S(180),FE-SI(180),BA- SI(180),AS-SI(180),MN- SI(180),NA-SI(180),PB- 6020S(180),AG-6020S(180),CR- SI(180),CA-SI(180),CD- 6020S(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) Project Name: Project Number: L1411620Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/13/14 Serial_No:06131415:12 Page 79 of 86 *Values in parentheses indicate holding time in days L1411620-07H L1411620-07I L1411620-07J L1411620-07K L1411620-08A Plastic 500ml unpreserved Plastic 250ml HNO3 preserved Amber 500ml unpreserved Amber 500ml unpreserved Vial HCl preserved A A A A B 8 <2 8 8 N/A 8.9 8.9 8.9 8.9 4.3 Y Y Y Y Y Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) HARDT(180) A2-1,4-DIOXANE-SIM(7) A2-1,4-DIOXANE-SIM(7) 8260(14) Project Name: Project Number: L1411620Lab Number: Report Date: L1411620-06E L1411620-07F Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 06/13/14 Container Comments Serial_No:06131415:12 Page 80 of 86 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1411620NANTUCKET LF 1910-97168-CG.SAMP 06/13/14 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Total: With respect to Organic analyses, a 'Total' result is defined as the summation of results for individual isomers or Aroclors. If a 'Total' result is requested, the results of its individual components will also be reported. This is applicable to 'Total' results for methods 8260, 8081 and 8082. Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:06131415:12 Page 81 of 86 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1411620NANTUCKET LF 1910-97168-CG.SAMP 06/13/14 Data Qualifiers H I M NJ P Q R RE S - - - - - - - - - The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The lower value for the two columns has been reported due to obvious interference. Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. Analytical results are from modified screening analysis. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:06131415:12 Page 82 of 86 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1411620NANTUCKET LF 1910-97168-CG.SAMP REFERENCES 06/13/14 Serial_No:06131415:12 Page 83 of 86 Certification Information Last revised April 15, 2014 The following analytes are not included in our NELAP Scope of Accreditation: Westborough Facility EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone (MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5-Trichlorobenzene, 4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260C: 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene, Iodomethane (methyl iodide), Methyl methacrylate, Azobenzene. EPA 8330A/B: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270D: 1-Methylnaphthalene, Dimethylnaphthalene,1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline, 4-Methylphenol. SM4500: Soil: Total Phosphorus, TKN, NO2, NO3. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Mansfield Facility EPA 8270D: Biphenyl. EPA 2540D: TSS EPA TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 1-Methylnaphthalene. The following analytes are included in our Massachusetts DEP Scope of Accreditation, Westborough Facility: Drinking Water EPA 200.8: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl; EPA 200.7: Ba,Be,Ca,Cd,Cr,Cu,Na; EPA 245.1: Mercury; EPA 300.0: Nitrate-N, Fluoride, Sulfate; EPA 353.2: Nitrate-N, Nitrite-N; SM4500NO3-F: Nitrate-N, Nitrite-N; SM4500F-C, SM4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, SM2320B, SM2540C, SM4500H-B EPA 332: Perchlorate. Microbiology: SM9215B; SM9223-P/A, SM9223B-Colilert-QT, Enterolert-QT. Non-Potable Water EPA 200.8: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn; EPA 200.7: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn; EPA 245.1, SM4500H,B, EPA 120.1, SM2510B, SM2540C, SM2340B, SM2320B, SM4500CL-E, SM4500F-BC, SM426C, SM4500NH3-BH, EPA 350.1: Ammonia-N, LACHAT 10-107-06-1-B: Ammonia-N, SM4500NO3-F, EPA 353.2: Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, SM4500P-B, E, SM5220D, EPA 410.4, SM5210B, SM5310C, SM4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. EPA 624: Volatile Halocarbons & Aromatics, EPA 608: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs EPA 625: SVOC (Acid/Base/Neutral Extractables), EPA 600/4-81-045: PCB-Oil. Microbiology: SM9223B-Colilert-QT; Enterolert-QT, SM9222D-MF. For a complete listing of analytes and methods, please contact your Alpha Project Manager. Serial_No:06131415:12 Page 84 of 86 Serial_No:06131415:12 Page 85 of 86 Serial_No:06131415:12 Page 86 of 86 Appendix D Landfill Gas Notification to MassDEP