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2013-10 Nantucket Landfill - Semi-Annual Environmental Monitoring Report
REPORT Summary of Groundwater, Surface Water and Landfill Gas Sampling Results Nantucket Landfill Nantucket, Massachusetts October 2013 Appendix A Site Plan Appendix B Sampling Results Summary Tables Table 1 Nantucket Landfill Nantucket, Massachusetts Groundwater Sampling Summary - October 2013 Water Levels Monitoring Well Number Sample Date Ground Elevation Top of PVC Elevation Well Depth (feet)PC2 PVC Difference3 Depth to Groundwater1 (feet) Elevation of Groundwater (feet) MW-1D 10/16/2013 21.06 23.21 75.96 2.47 0.32 19.29 3.92 MW-1S 10/16/2013 20.71 22.84 26.52 2.46 0.33 19.62 3.22 MW-3D 10/15/2013 5.53 7.66 71.73 2.37 0.24 5.42 2.24 MW-3S 10/15/2013 5.35 7.39 12.71 2.63 0.59 5.39 2.00 MW-4D NM 4 NA 5.36 NA NA NA NM NA MW-4S NM 4 NA 4.61 NA NA NA NM NA MW-5D 10/16/2013 7.38 9.79 62.27 2.41 0.00 8.42 1.37 MW-5S 10/16/2013 7.82 10.36 13.73 2.75 0.21 8.46 1.90 MW-6D 10/16/2013 8.26 11.10 62.36 2.78 -0.06 8.42 2.68 MW-6S 10/16/2013 9.03 10.54 14.74 1.63 0.12 7.92 2.62 MW-7D 10/15/2013 6.79 7.59 60.83 0.76 -0.04 5.42 2.17 MW-7S 10/15/2013 6.70 7.45 15.04 1.02 0.27 5.91 1.54 MW-8D 10/16/2013 NM 7.36 42.22 1.75 0.05 4.26 3.10 MW-8S 10/16/2013 NM 6.55 15.32 2.54 0.23 3.58 2.97 Notes: (1) Depth to water measured from top of PVC (2) PC = Height of protective casing measured from the ground surface (3) PVC Difference = Measured distance between the top of the PVC and the top of the protective casing (4) MW-4S and MW-4D have been buried in fill material and are no longer accessible for sampling NM = Not Measured TOC = Top of Casing NA = Not Available Table 2 Nantucket Landfill Nantucket, Massachusetts Groundwater Sampling Summary - October 2013 Metals, Field Parameters, and Indicator Parameters MW-1D MW-1S MW-3D DUP-1 MW-3S MW-5D MW-5S MW-6D MW-6S MW-7D MW-7S MW-8D MW-8S L1320833-04 L1320833-03 L1320693-02 L1320693-05 L1320693-01 L1320833-08 L1320833-07 L1320833-06 L1320833-05 L1320693-04 L1320693-03 L1320833-02 L1320833-01 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 Drinking Water Standards Units Field Parameters Temperature NL ºC 11.11 12.56 12.45 --15.35 12.50 15.39 11.79 16.56 12.94 15.93 15.75 11.34 Specific Conductivity NL us/cmc 122 95 625 --829 255 135 100 208 305 994 373 73 Dissolved Oxygen NL mg/l 6.24 5.48 2.04 --0.65 2.51 2.14 3.59 2.70 1.20 0.54 0.27 6.12 pH 6.5-8.4 (3,5)std units 6.67 6.13 6.25 --6.18 6.03 5.08 5.28 5.54 6.04 6.64 6.07 5.36 Indicator Parameters Alkalinity NL mg/l 44.9 3.70 221 228 315 25.2 <2.00 7.60 6.20 74.1 384 6.40 128 TDS (Tot. Dissolved Solids)500 (3,5)mg/l 86 53 440 460 630 180 89 70 120 270 680 40 290 Nitrate-Nitrogen 10 (2,4)mg/l 0.273 <0.100 <0.100 <0.100 <0.100 <0.100 0.204 1.09 6.47 <0.100 <0.100 0.704 <0.100 Cyanide, Total 0.2(4)mg/l <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.005 <0.005 <0.005 Sulfate 250(3,5)mg/l <10 <10 63 61 <50 16 <10 <10 16 51 140 <10 <20 Chloride 250(3,5)mg/l 16 29 70 72 110 63 37 25 43 37 60 17 49 COD (Chemical Oxygen Demand )NL mg/l <20 <20 41 29 130 <20 <20 <20 <20 <20 73 <20 80 Dissolved Metals Arsenic 10 (2,4)ug/l <5.0 <5.0 <5.0 <5.0 14.8 <5.0 <5.0 <5.0 <5.0 <5.0 39 <5.0 14.3 Barium 2,000 (2,4)ug/l <10.0 <10.0 27.8 26.8 50.9 <10.0 37.3 <10.0 88.1 11.7 42.7 <10.0 20.9 Cadmium 5 (2,4)ug/l <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 <5.0 Calcium NL ug/l 16,000 1,800 47,000 45,000 67,000 7,300 1,700 3,500 13,000 20,000 120,000 1,900 30,000 Chromium 100 (2,4)ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 Copper 1,300 (2,4)ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 Iron 300 (3,5)ug/l <50.0 <50.0 240 230 22,000 <50.0 1,300 <50.0 <50.0 1,000 41,000 <50.0 5,100 Lead 15 (2,4)ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 Manganese 50 (3,5)ug/l <10.0 <10.0 1,250 1,200 306.0 598 236 <10.0 269 83.0 941 <10.0 375 Mercury 2 (2,4)ug/l <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 <0.20 Selenium 50 (2,4)ug/l <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 <10.0 Silver 100 (3,5)ug/l <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 <7.0 Sodium 20,000 (3)ug/l 12,000 16,000 73,000 70,000 83,000 45,000 23,000 16,000 23,000 25,000 56,000 11,000 40,000 Zinc 5,000 (3,5)ug/l <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 <50.0 103 <50.0 <50.0 (8) Initial and final readings were collected for field parameters; final readings are presented. Sample Location Laboratory ID Sample Date NL: No Limit Notes: (1) Highlighted Areas: Concentration Equals or Exceeds Massachusetts or EPA Drinking Water Standards or Guidelines (2) Massachusetts Drinking Water Standard or Maximum Contaminant Level (MCL); Version Spring 2012. (3) Massachusetts Drinking Water Guideline Or Secondary Maximum Contaminant Level (SMCL); Version Spring 2012. (4) EPA Primary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm (5) EPA Secondary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm (6) DUP-1 taken at MW-3D <#.# Not detected to the limit indicated (7) Samples could not be taken from wells MW-4S and MW-4D as they have been filled over. Table 3 Continued Nantucket Landfill Nantucket, Massachusetts Groundwater Sampling Summary - October 2013 Volatile Organic Compounds Continued Table 3 Nantucket Landfill Nantucket, Massachusetts Groundwater Sampling Summary - October 2013 Volatile Organic Compounds MW-1D MW-1S MW-3D DUP-1 MW-3S MW-5D MW-5S MW-6D MW-6S MW-7D MW-7S MW-8D MW-8S L1320833-04 L1320833-03 L1320693-02 L1320693-05 L1320693-01 L1320833-08 L1320833-07 L1320833-06 L1320833-05 L1320693-04 L1320693-03 L1320833-02 L1320833-01 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 Drinking Water Standards Units Volatile Organic Compounds 1,1,1,2-Tetrachloroethane NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,1,1-Trichloroethane 200 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,1,2,2-Tetrachloroethane NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,1,2-Trichloroethane 5 (2,4)ug/l <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 1,1-Dichloroethane 70 (3)ug/l <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 1,1-Dichloroethene 7 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,1-Dichloropropene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2,3- Trichlorobenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2,3-Trichloropropane NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 1,2,4-Trichlorobenzene 70 (2,4)ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2,4-Trimethylbenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2- Dibromo-3-Chloropropane 0.2 (2,4)ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2-Dibromoethane 0.02 (2)ug/l <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 1,2-Dichlorobenzene 600 (2,4)ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,2-Dichloroethane 5 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1,2-Dichloropropane 5 (2,4)ug/l <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 1,3,5-Trimethylbenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,3-Dichlorobenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,3-Dichloropropane NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,4-Dichlorobenzene 5 (2)ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 1,4-Dichlorobutane NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 1,4-Dioxane 0.3 (3)ug/l <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 <250 2,2-Dichloropropane NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 2-Butanone 4000 (3)ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 2-Chlorotoluene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 2-Hexanone NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 4-Chlorotoluene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 4-Methyl-2-Pentanone 350 (3)ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Acetone 6300 (3)ug/l <5 <5 <5 <5 6.2 <5 <5 <5 <5 <5 <5 <5 <5 Acrylonitrile NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Benzene 5 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.4 <0.5 <0.5 Bromobenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Bromochloromethane NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Bromodichloromethane NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bromoform NL ug/l <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Bromomethane 10 (3)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Carbon Disulfide NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Carbon Tetrachloride 5 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Chlorobenzene 100 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 0.66 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Chloroethane NL ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Chloroform 70 (3)ug/l <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 Chloromethane NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 cis 1,2-Dichloroethene 70 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 cis 1,3-Dichloropropene 0.4 (3)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dibromochloromethane NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dibromomethane NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Dichlorodifluoromethane 1400 (3)ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Ethylbenzene 700 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Ethyl Ether NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Ethyl Methacrylate NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Hexachlorobutadiene NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Isopropylbenzene NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 p-Isopropytoluene NL ug/l <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 m- and p- Xylenes 10,000 (tot. xylenes)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Methyl Tert-Butyl Ether 70 (3)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Methylene Chloride 5 (2,4)ug/l <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 Sample Location Laboratory ID Sample Date Table 3 Continued Nantucket Landfill Nantucket, Massachusetts Groundwater Sampling Summary - October 2013 Volatile Organic Compounds Continued MW-1D MW-1S MW-3D DUP-1 MW-3S MW-5D MW-5S MW-6D MW-6S MW-7D MW-7S MW-8D MW-8S L1320833-04 L1320833-03 L1320693-02 L1320693-05 L1320693-01 L1320833-08 L1320833-07 L1320833-06 L1320833-05 L1320693-04 L1320693-03 L1320833-02 L1320833-01 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 10/16/2013 10/16/2013 10/15/2013 10/15/2013 10/16/2013 10/16/2013 Drinking Water Standards Units Sample Location Laboratory ID Sample Date n-Butylbenzene NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 n-Propylbenzene NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Naphthalene 140 (3)ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 o-Xylene 10,000 (tot. xylenes)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 sec-Butylbenzene NL ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Styrene 100 (2,4)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 tert-Butylbenzene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Tetrachloroethene 5 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Tetrahydrofuran 1300 (3)ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Toluene 1000 (2,4)ug/l <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 trans-1,2-Dichloroethene 100 (2,4)ug/l <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <0.75 trans-1,3-Dichloropropene 0.4 (3)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 trans-1,4-Dichloro-2-butene NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Trichloroethene 5 (2,4)ug/l <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Trichlorofluoromethane NL ug/l <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Vinyl acetate NL ug/l <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Vinyl Chloride 2 (2,4)ug/l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Notes: (1) Highlighted Areas: Concentration Equals or Exceeds Massachusetts or EPA Drinking Water Standards or Guidelines (2) Massachusetts Drinking Water Standard Or Maximum Contaminant Level (MCL); Version Spring 2012. (3) Massachusetts Drinking Water Guideline Or Secondary Maximum Contaminant Level (SMCL); Version Spring 2012. (4) EPA Primary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm (5) EPA Secondary Drinking Water Standard, as found at: http://water.epa.gov/drink/contaminants/index.cfm <#.# Not Detected to the limit indicated NL: No Limit (6) DUP-1 taken at MW-3D Table 4 Nantucket Landfill Nantucket, Massachusetts Surface Water Sampling Summary - October 2013 Metals, Field Parameters, Indicator Parameters SW-1 SW-2 SW-3 L1320693-06 NS NS 10/15/2013 NS NS NRWQC2,3 Units Field Parameters Temperature NL ºC 18.31 NS NS Specific Conductivity NL us/cmc 29,053 NS NS Dissolved Oxygen NL mg/L 5.03 NS NS pH 6.5-9 standard units 7.07 NS NS Indicator Parameters Alkalinity 20 mg/L 63.5 NS NS Chloride 230 mg/L 8,900 NS NS COD (Chemical Oxygen Demand)NL mg/L 720 NS NS Cyanide, Total 0.0052 mg/L <0.005 NS NS Nitrate-Nitrogen NL mg/L <0.100 NS NS Sulfate NL mg/L 1,400 NS NS TDS (Total Dissolved Solids)NL mg/L 19,000 NS NS Measured Hardness NL mg/L 2,300 NS NS Dissolved Metals NS NS Arsenic 150 ug/L <5.0 NS NS Barium NL ug/L 18.2 NS NS Cadmium 2.154,5 ug/L <0.40 NS NS Calcium NL ug/L 210,000 NS NS Chromium 74 6 ug/L <10 NS NS Copper 130.54,5 ug/L <2.00 NS NS Iron 1,000 ug/L <50 NS NS Lead 57.54,5 ug/L <10.00 NS NS Manganese NL ug/L 78.7 NS NS Mercury 0.77 ug/L <0.20 NS NS Selenium 5 ug/L <10.0 NS NS Silver 7074,5 ug/L <0.80 NS NS Sodium NL ug/L 3,100,000 NS NS Zinc 1,6834,5 ug/L <50.0 NS NS Notes: (1) Highlighted Areas: Concentration Equals or Exceeds NRWQC (2) NRWQC: National Recommended Water Quality Criteria for Freshwater Based Surface Water, Version 2009 Maximum Concentrations (CMC) values are used Appendix B of the NRWQC Guidance Document (5) See Table 4A for the individual hardness dependent criteria for each sampling location Chromium results represent total chromium, however total chromium is generally assumed to be representative of chromium III, therefore the total chromium results are compared to the chromium III NRWQC (7) Initial and final readings were collected for field parameters; final readings are presented. <#.# Not detected to the limit indicated NL: No Limit NS: Not Sampled (6) The NRWQC has established hardness dependent criteria for chromium III and chromium IV. (4) This NRWQC is hardness dependent and is calculated based upon the equations and factors presented in (3) Criterion continuous conentrations (CCC) values are compared to unless none are available, Criterion Sample Location Laboratory ID Sample Date Table 4A Nantucket Landfill Nantucket, Massachusetts Surface Water Sampling Summary - October 2013 Calculated NRWQC for Hardness Dependent Metals Surface Water Sampling Locations Measured Hardness (mg/L) October 2013 Cadmium Value (ug/L) Calculated Cadmium Criteria (ug/L) October 2013 Copper Value (ug/L) Calculated Copper Criteria (ug/L) October 2013 Lead Value (ug/L) Calculated Lead Criteria (ug/L) October 2013 Silver Value (ug/L) Calculated Silver Criteria (ug/L) October 2013 Zinc Value (ug/L) Calculated Zinc Criteria (ug/L) SW-1 2,300 <0.40 2.15 <2.00 130.5 <10.00 57.5 <0.80 707 <50.0 1,683 SW-2 NS NS NS NS NS NS NS NS NS NS NS SW-3 NS NS NS NS NS NS NS NS NS NS NS Notes: <#.# Not detected to the limit indicated (1) Hardness dependent metals require the NRWQC to be calculated if the sample hardness differs from 100 mg/L. Criteria are calcuated according to the equations and factors presented in Appendix B of the NRWQC Guidance Document dated 2009. (2) Highlighted areas: Concentration equals or exceeds calculated hardness dependent NRWQC. Table 5 Nantucket Landfill Nantucket, Massachusetts Surface Water Sampling Summary - October 2013 Volatile Organic Compounds SW-1 SW-2 SW-3 L1320693-06 NS NS 10/15/2013 NS NS NRWQC2,3 Units Volatile Organic Compounds 1,1,1,2-Tetrachloroethane NL ug/L <0.5 NS NS 1,1,1-Trichloroethane NL ug/L <0.5 NS NS 1,1,2,2-Tetrachloroethane NL ug/L <0.5 NS NS 1,1,2-Trichloroethane NL ug/L <0.75 NS NS 1,1-Dichloroethane NL ug/L <0.75 NS NS 1,1-Dichloroethene NL ug/L <0.5 NS NS 1,1-Dichloropropene NL ug/L <2.5 NS NS 1,2,3- Trichlorobenzene NL ug/L <2.5 NS NS 1,2,3-Trichloropropane NL ug/L <5 NS NS 1,2,4-Trichlorobenzene NL ug/L <2.5 NS NS 1,2,4-Trimethylbenzene NL ug/L <2.5 NS NS 1,2- Dibromo-3-Chloropropane NL ug/L <2.5 NS NS 1,2-Dibromoethane NL ug/L <2 NS NS 1,2-Dichlorobenzene NL ug/L <2.5 NS NS 1,2-Dichloroethane NL ug/L <0.5 NS NS 1,2-Dichloropropane NL ug/L <1.8 NS NS 1,3,5-Trimethylbenzene NL ug/L <2.5 NS NS 1,3-Dichlorobenzene NL ug/L <2.5 NS NS 1,3-Dichloropropane NL ug/L <2.5 NS NS 1,4-Dichlorobenzene NL ug/L <2.5 NS NS 1,4-Dichlorobutane NL ug/L <5 NS NS 1,4-Dioxane NL ug/L <250 NS NS 2,2-Dichloropropane NL ug/L <2.5 NS NS 2-Butanone NL ug/L <5 NS NS 2-Chlorotoluene NL ug/L <2.5 NS NS 2-Hexanone NL ug/L <5 NS NS 4-Chlorotoluene NL ug/L <2.5 NS NS 4-Methyl-2-Pentanone NL ug/L <5 NS NS Acetone NL ug/L <5 NS NS Acrylonitrile NL ug/L <5 NS NS Benzene NL ug/L <0.5 NS NS Bromobenzene NL ug/L <2.5 NS NS Bromochloromethane NL ug/L <2.5 NS NS Bromodichloromethane NL ug/L <0.5 NS NS Bromoform NL ug/L <2 NS NS Bromomethane NL ug/L <1 NS NS Carbon Disulfide NL ug/L <5 NS NS Carbon Tetrachloride NL ug/L <0.5 NS NS Chlorobenzene NL ug/L <0.5 NS NS Chloroethane NL ug/L <1 NS NS Chloroform NL ug/L <0.75 NS NS Chloromethane NL ug/L <2.5 NS NS cis 1,2-Dichloroethene NL ug/L <0.5 NS NS cis 1,3-Dichloropropene NL ug/L <0.5 NS NS Dibromochloromethane NL ug/L <0.5 NS NS Dibromomethane NL ug/L <5 NS NS Dichlorodifluoromethane NL ug/L <5 NS NS Ethylbenzene NL ug/L <0.5 NS NS Ethyl Ether NL ug/L <2.5 NS NS Ethyl Methacrylate NL ug/L <5 NS NS Hexachlorobutadiene NL ug/L <0.5 NS NS Isopropylbenzene NL ug/L <0.5 NS NS p-Isopropyltoluene NL ug/L <0.5 NS NS m- and p- Xylenes NL ug/L <1 NS NS Methyl Tert-Butyl Ether NL ug/L <1 NS NS Methylene Chloride NL ug/L <3 NS NS n-Butylbenzene NL ug/L <0.5 NS NS n-Propylbenzene NL ug/L <0.5 NS NS Naphthalene NL ug/L <2.5 NS NS o-Xylene NL ug/L <1 NS NS sec-Butylbenzene NL ug/L <0.5 NS NS Styrene NL ug/L <1 NS NS tert-Butylbenzene NL ug/L <2.5 NS NS Tetrachloroethene NL ug/L <0.5 NS NS Tetrahydrofuran NL ug/L <5 NS NS Toluene NL ug/L <0.75 NS NS trans-1,2-Dichloroethene NL ug/L <0.75 NS NS trans-1,3-Dichloropropene NL ug/L <0.5 NS NS trans-1,4-Dichloro-2-butene NL ug/L <2.5 NS NS Trichloroethene NL ug/L <0.5 NS NS Trichlorofluoromethane NL ug/L <2.5 NS NS Vinyl acetate NL ug/L <5 NS NS Vinyl Chloride NL ug/L <1 NS NS Notes: (1) Highlighted Areas: Concentration Equals or Exceeds NRWQC (2) NRWQC: National Recommended Water Quality Criteria for Freshwater Based Surface Water, Version 2009 (3) Criterion continuous concentrations (CCC) values are compared to unless none are available, Criterion Maximum Concentrations (CMC) values are used <#.# Not detected to the limit indicated NL: No Limit Sample Location Laboratory ID Sample Date Table 6 Nantucket Landfill Nantucket, Massachusetts Landfill Gas Sampling Summary -October 2013 LEL (%) Initial Final Initial Final Initial Final Initial Final Initial Final Initial Final LGW-1 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.2 0.4 20.8 20.6 29.84 LGW-2 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.8 0.9 20.2 20.8 29.88 LGW-3 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.9 1.0 20.0 20.0 29.88 LGW-4 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.5 0.5 20.5 20.5 29.88 LGW-5 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 4.3 2.0 14.8 18.2 29.88 LGW-6 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.4 4.0 20.3 15.5 29.88 LGW-7 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 2.0 2.4 19.3 19.0 29.88 LGW-8 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.6 0.3 20.0 20.3 29.90 LGW-9 Well 10/17/2013 0.0 0.0 0.0 0.0 0.2 0.2 4 4 0.3 0.4 20.6 20.5 29.90 LGW-10 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.5 0.5 20.5 20.5 29.88 LGW-11 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.4 0.1 20.4 20.8 29.88 LGW-12 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 1.4 1.5 19.7 19.6 29.88 LGW-13 Well 10/17/2013 0.0 0.0 0.0 0.0 0.0 0.0 0 0 0.0 0.0 20.8 20.9 29.88 LGW-14 Well 10/17/2013 2.4 2.5 9.0 9.4 56.8 57.3 1136 1146 29.6 29.8 0.5 0.3 29.88 LGW-15 Well 10/17/2013 2.4 2.4 1.3 1.2 57.9 59.0 0 0 30.1 31.0 1.2 0.3 29.88 LGW-16 Well 10/17/2013 3.3 3.4 0.3 0.3 55.5 55.7 0 0 30.4 30.6 0.4 0.2 29.88 LGW-17 Well 10/17/2013 1.9 2.0 17.2 17.4 57.2 57.4 0 0 35.9 36.1 0.3 0.1 29.88 LGW-18 Well 10/17/2013 3.7 3.7 0.0 0.0 47.5 38.9 0 0 38.8 35.5 0.2 1.4 29.88 Notes: (1) Probes and wells were purged for approximately 10 minutes before final readings were recorded. (2) Methane, oxygen and carbon dioxide, measured with GEM-2000 combustible gas meter. (3) Volatile Organic Compounds (VOCs) measured with an Organic Vapor Meter (OVM), lamp eV 10.6. (4) Hydrogen Sulfide measured with an Interscan1000 meter. NS= Not Sampled Gas Monitoring Locations H2S (ppm)CH4 (% by Vol.)CO2 (%)Barometric Pressure (In. Hg) O2 (%)VOCs (ppmv)Type Date Appendix C Laboratory Reports and Chains of Custody L1320693 CDM Smith, Inc. 1910-97168-CG.SAMP NANTUCKET LF Client: Project Name: Project Number: 10/30/13 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:10301320:59 Page 1 of 77 L1320693-01 L1320693-02 L1320693-03 L1320693-04 L1320693-05 L1320693-06 L1320693-07 L1320693-08 Alpha Sample ID MW-3S MW-3D MW-7S MW-7D DUP-1 SW-1 FB-1 TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320693 10/30/13 10/15/13 14:00 10/15/13 14:00 10/15/13 14:40 10/15/13 15:10 10/15/13 00:00 10/15/13 15:00 10/15/13 15:00 10/15/13 00:00 Collection Date/Time Serial_No:10301320:59 Page 2 of 77 NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320693 10/30/13 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Serial_No:10301320:59 Page 3 of 77 Case Narrative (continued) NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320693 10/30/13 Sample Receipt L1320693-01 through -07 were field filtered for Dissolved Metals. Total Metals L1320693-06 has elevated detection limits for cadmium, copper, lead and silver due to the dilutions required by matrix interferences encountered during analysis. The WG647255-4 MS recoveries for calcium (70%) and sodium (70%), performed on L1320693-02, do not apply because the sample concentrations are greater than four times the spike amounts added. Sulfate L1320693-01 has an elevated detection limit due to the dilution required by the sample matrix. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 10/30/13 Serial_No:10301320:59 Page 4 of 77 ORGANICS Serial_No:10301320:59 Page 5 of 77 VOLATILES Serial_No:10301320:59 Page 6 of 77 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND 0.66 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 MW-3SClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 16:16 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 7 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND 6.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 MW-3SClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 8 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 108 95 97 101 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 MW-3SClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 9 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 MW-3DClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 16:56 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 10 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 MW-3DClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 11 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 107 94 99 101 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 MW-3DClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 12 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.4 ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 MW-7SClient ID: 10/15/13 14:40Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 17:35 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 13 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 MW-7SClient ID: 10/15/13 14:40Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 14 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 105 95 96 99 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 MW-7SClient ID: 10/15/13 14:40Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 15 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 MW-7DClient ID: 10/15/13 15:10Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 18:14 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 16 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 MW-7DClient ID: 10/15/13 15:10Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 17 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 109 96 99 104 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 MW-7DClient ID: 10/15/13 15:10Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 18 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 DUP-1Client ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 18:53 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 19 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 DUP-1Client ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 20 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 109 94 100 103 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 DUP-1Client ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 21 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 SW-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 19:30 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 22 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 SW-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 23 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 114 95 98 103 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 SW-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 24 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 FB-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 20:07 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 25 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 FB-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 26 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 106 97 98 101 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 FB-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10301320:59 Page 27 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/30/13 TRIP BLANKClient ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-08Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 20:44 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 28 of 77 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/30/13 TRIP BLANKClient ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-08Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 29 of 77 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 106 96 100 102 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/30/13 TRIP BLANKClient ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: NANTUCKET, MASample Location: L1320693-08Lab ID: Field Prep:Not Specified MDL -- -- -- -- Serial_No:10301320:59 Page 30 of 77 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/21/13 11:06 1,8260CAnalytical Method: Analytical Date: 10/30/13 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG645688-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 31 of 77 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/21/13 11:06 1,8260CAnalytical Method: Analytical Date: 10/30/13 Analyst:PD Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG645688-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 32 of 77 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/21/13 11:06 1,8260CAnalytical Method: Analytical Date: 10/30/13 Analyst:PD Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND RL 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-08 Batch: WG645688-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 98 98 103 98 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 33 of 77 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 104 103 92 90 108 96 108 95 98 82 91 87 95 102 96 96 93 111 101 99 98 108 105 94 89 109 95 109 97 101 85 92 87 95 102 94 96 91 113 103 103 101 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 4 2 2 1 1 1 1 2 3 4 1 0 0 0 2 0 2 2 2 4 3 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG645688-1 WG645688-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Qual Qual Serial_No:10301320:59 Page 34 of 77 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 81 43 75 98 93 99 93 99 98 96 90 100 101 97 98 113 103 102 79 160 108 86 40 77 103 98 100 92 101 101 100 87 103 104 100 99 113 105 104 83 169 115 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 6 7 3 5 5 1 1 2 3 4 3 3 3 3 1 0 2 2 5 5 6 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG645688-1 WG645688-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Qual Q Q Qual Serial_No:10301320:59 Page 35 of 77 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 150 119 105 120 103 133 99 129 98 96 102 99 97 98 100 97 97 96 98 90 96 147 111 100 117 101 132 98 122 99 95 103 101 98 104 105 101 98 100 93 97 98 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 2 7 5 3 2 1 1 6 1 1 1 2 1 6 5 4 1 4 5 7 2 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG645688-1 WG645688-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Qual Q Q Q Q Qual Serial_No:10301320:59 Page 36 of 77 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 97 93 101 93 87 96 97 104 88 126 102 92 105 93 88 101 101 102 90 121 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 5 1 4 0 1 5 4 2 2 4 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-08 Batch: WG645688-1 WG645688-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 94 97 95 97 70-130 70-130 70-130 70-130 94 98 94 96 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 10/30/13 Acceptance Criteria Qual Qual Qual Serial_No:10301320:59 Page 37 of 77 METALS Serial_No:10301320:59 Page 38 of 77 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS MW-3SClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 0.0148 0.0509 ND 67. ND ND 22. ND 0.306 ND ND ND 83. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/25/13 11:51 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 10/29/13 19:43 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 39 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS MW-3DClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0278 ND 47. ND ND 0.24 ND 1.25 ND ND ND 73. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/25/13 11:53 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 10/29/13 19:28 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 40 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS MW-7SClient ID: 10/15/13 14:40Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 0.0390 0.0427 ND 120 ND ND 41. ND 0.941 ND ND ND 56. 0.103 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/25/13 11:55 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 10/29/13 19:47 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 41 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS MW-7DClient ID: 10/15/13 15:10Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0117 ND 20. ND ND 1.0 ND 0.0830 ND ND ND 25. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/25/13 11:56 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 10/29/13 20:03 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 42 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS DUP-1Client ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0268 ND 45. ND ND 0.23 ND 1.20 ND ND ND 70. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/25/13 11:58 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 10/29/13 20:06 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 43 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS SW-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Total Hardness by SM 2340B - Westborough Lab Dissolved Metals - Westborough Lab Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 2300 ND 0.0182 ND 210 ND ND ND ND 0.0787 ND ND ND 3100 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 2 1 1 2 1 10 1 1 1 2 1 1 0.66 0.0050 0.0100 0.00040 0.10 0.010 0.00200 0.050 0.01000 0.0100 0.00020 0.0100 0.00080 2.0 0.0500 10/30/13 16:25 10/29/13 20:10 10/29/13 20:10 10/29/13 16:02 10/29/13 20:10 10/29/13 20:10 10/29/13 16:02 10/29/13 20:10 10/29/13 16:10 10/29/13 20:10 10/25/13 12:00 10/29/13 20:10 10/29/13 16:02 10/29/13 20:10 10/29/13 20:10 1,6010C 1,6010C 1,6010C 1,6020A 1,6010C 1,6010C 1,6020A 1,6010C 1,6020A 1,6010C 1,7470A 1,6010C 1,6020A 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/29/13 11:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 EPA 3005A NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 44 of 77 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 SAMPLE RESULTS FB-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320693-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/25/13 12:02 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 10/29/13 20:14 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 45 of 77 FF Parameter Parameter Parameter Result Result Result Dilution Factor Dilution Factor Dilution Factor Qualifier Qualifier Qualifier Units Units Units RL RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Date Analyzed Date Analyzed Date Analyzed Analytical Method Analytical Method Analytical Method Analyst Analyst Analyst Date Prepared Date Prepared Date Prepared 10/30/13 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.00020 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 0.00020 0.00100 0.00100 0.00040 10/25/13 11:43 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 19:20 10/29/13 14:01 10/29/13 14:01 10/29/13 14:01 10/29/13 14:01 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6020A 1,6020A 1,6020A 1,6020A DR KL KL KL KL KL KL KL KL KL KL KL KL KL KL KL KL KL 10/25/13 08:01 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 10/26/13 12:39 Dissolved Metals - Westborough Lab for sample(s): 01-07 Batch: WG646884-1 Dissolved Metals - Westborough Lab for sample(s): 01-07 Batch: WG647255-1 Dissolved Metals - Westborough Lab for sample(s): 06 Batch: WG647808-1 EPA 7470A NA Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10301320:59 Page 46 of 77 Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Date Analyzed Analytical Method Analyst Date Prepared 10/30/13 Hardness ND mg/l 10.66 10/30/13 15:50 1,6010C KL10/29/13 11:39 Total Hardness by SM 2340B - Westborough Lab for sample(s): 06 Batch: WG647817-1 NA EPA 3005A Digestion Method: Digestion Method: Prep Information Prep Information MDL NA Serial_No:10301320:59 Page 47 of 77 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 98 102 102 102 99 100 102 100 104 99 105 106 100 100 - - - - - - - - - - - - - - 70-130 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-07 Batch: WG646884-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-07 Batch: WG647255-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Qual Qual Serial_No:10301320:59 Page 48 of 77 Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Hardness 104 95 97 92 97 - - - - - 80-120 80-120 80-120 80-120 80-120 - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 06 Batch: WG647808-2 Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 06 Batch: WG647817-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Serial_No:10301320:59 Page 49 of 77 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved ND ND 0.0278 ND 47 ND ND 0.24 ND 1.25 ND ND 73 ND ND ND ND ND 0.00583 0.127 2.02 0.0510 54 0.20 0.262 1.2 0.505 1.67 0.130 0.0514 80 0.501 0.05202 0.2351 0.4873 0.04029 117 106 100 100 70 100 105 96 99 84 108 103 70 100 102 94 96 80 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 70-130 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646884-4 QC Sample: L1321233-01 Client ID: MS Sample Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG647255-4 QC Sample: L1320693-02 Client ID: MW-3D Dissolved Metals - Westborough Lab Associated sample(s): 06 QC Batch ID: WG647808-4 QC Sample: L1319435-74 Client ID: MS Sample 0.005 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 0.051 0.25 0.51 0.05 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Q Q Qual Qual Serial_No:10301320:59 Page 50 of 77 Hardness 82 140 88 --75-125 -20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 06 QC Batch ID: WG647817-4 QC Sample: L1321456-09 Client ID: MS Sample 66.2 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Serial_No:10301320:59 Page 51 of 77 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND 0.0278 ND 47 ND ND 0.24 ND 1.25 ND ND 73 ND ND ND 0.0277 ND 46. ND ND 0.23 ND 1.24 ND ND 73. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l NC NC 0 NC 2 NC NC 4 NC 1 NC NC 0 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646884-3 QC Sample: L1321233-01 Client ID: DUP Sample Dissolved Metals - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG647255-3 QC Sample: L1320693-02 Client ID: MW-3D NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1320693Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 10/30/13 Qual Serial_No:10301320:59 Page 52 of 77 Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l NC NC NC NC 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 06 QC Batch ID: WG647808-3 QC Sample: L1319435-74 Client ID: DUP Sample NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1320693Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 10/30/13 Serial_No:10301320:59 Page 53 of 77 INORGANICS & MISCELLANEOUS Serial_No:10301320:59 Page 54 of 77 FF MW-3SClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 315. 630 ND 110 ND ND 130 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 5 1 5 1 2.00 10 0.005 5.0 0.100 50 20 10/23/13 16:58 10/18/13 07:35 10/28/13 12:57 10/17/13 11:24 10/17/13 00:59 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 55 of 77 FF MW-3DClient ID: 10/15/13 14:00Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 221. 440 ND 70. ND 63. 41. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 10/23/13 16:58 10/18/13 07:35 10/28/13 12:58 10/17/13 11:25 10/17/13 01:00 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 56 of 77 FF MW-7SClient ID: 10/15/13 14:40Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 384. 680 0.005 60. ND 140 73. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 5 1 2.00 10 0.005 1.0 0.100 50 20 10/23/13 16:58 10/18/13 07:35 10/28/13 12:59 10/17/13 11:00 10/17/13 01:01 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 57 of 77 FF MW-7DClient ID: 10/15/13 15:10Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 74.1 270 ND 37. ND 51. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 10/23/13 16:58 10/21/13 10:20 10/28/13 13:00 10/17/13 11:01 10/17/13 01:01 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 58 of 77 FF DUP-1Client ID: 10/15/13 00:00Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 228. 460 ND 72. ND 61. 29. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 10/23/13 16:58 10/21/13 10:20 10/28/13 13:02 10/17/13 11:02 10/17/13 01:02 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 59 of 77 FF SW-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 63.5 19000 ND 8900 ND 1400 720 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 100 1 100 1 2.00 10 0.005 100 0.100 1000 20 10/23/13 16:58 10/21/13 10:20 10/28/13 13:03 10/17/13 11:27 10/17/13 01:03 10/23/13 14:15 10/22/13 17:02 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 60 of 77 FF FB-1Client ID: 10/15/13 15:00Date Collected: 10/16/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320693-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand ND ND ND ND ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/23/13 16:58 10/21/13 10:20 10/28/13 13:05 10/17/13 11:28 10/17/13 01:03 10/23/13 14:15 10/22/13 17:03 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 08:30 - - 10/23/13 14:15 10/22/13 14:00 10/30/13 MDL NA -- -- -- -- -- -- Serial_No:10301320:59 Page 61 of 77 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 Date Analyzed Analytical Method Analyst Date Prepared 10/30/13 Nitrogen, Nitrate Chloride Solids, Total Dissolved Solids, Total Dissolved Chemical Oxygen Demand Sulfate Alkalinity, Total Cyanide, Total ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg CaCO3/L mg/l 1 1 1 1 1 1 1 1 0.100 1.0 10 10 20 10 2.00 0.005 10/17/13 00:45 10/17/13 10:38 10/18/13 07:35 10/21/13 10:20 10/22/13 16:59 10/23/13 14:15 10/23/13 16:58 10/28/13 12:48 30,4500NO3-F 1,9251 30,2540C 30,2540C 30,5220D 1,9038 30,2320B 1,9010C/9012A DB LA DW DW TL MP SP JO - - - - 10/22/13 14:00 10/23/13 14:15 - 10/25/13 08:30 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG644565-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG644662-1 General Chemistry - Westborough Lab for sample(s): 01-03 Batch: WG644982-1 General Chemistry - Westborough Lab for sample(s): 04-07 Batch: WG645493-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG645946-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG646289-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG646457-1 General Chemistry - Westborough Lab for sample(s): 01-07 Batch: WG646909-1 MDL -- -- -- -- -- -- NA -- Serial_No:10301320:59 Page 62 of 77 Nitrogen, Nitrate Chloride Solids, Total Dissolved Solids, Total Dissolved Chemical Oxygen Demand Sulfate Alkalinity, Total 101 97 92 104 101 90 104 - - - - - - - 90-110 90-110 80-120 80-120 93-106 84-119 90-110 - - - - - - -10 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG644565-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG644662-2 General Chemistry - Westborough Lab Associated sample(s): 01-03 Batch: WG644982-2 General Chemistry - Westborough Lab Associated sample(s): 04-07 Batch: WG645493-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG645946-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG646289-2 General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG646457-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Qual Qual Serial_No:10301320:59 Page 63 of 77 Cyanide, Total 105 105 80-120 0 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 Batch: WG646909-2 WG646909-3 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Serial_No:10301320:59 Page 64 of 77 Nitrogen, Nitrate Chloride Chemical Oxygen Demand Sulfate Alkalinity, Total Cyanide, Total 1.05 10 89 ND 74.1 ND 4.90 30 330 30 176 0.207 96 100 102 150 102 104 - - - - - 0.207 - - - - - 104 83-113 58-140 84-120 55-147 86-116 80-120 - - - - - 0 17 7 12 14 10 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG644565-4 QC Sample: L1320740-03 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG644662-4 QC Sample: L1320765-05 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG645946-3 QC Sample: L1320974-07 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646289-4 QC Sample: L1321297-02 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646457-4 QC Sample: L1320693-04 Client ID: MW-7D General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646909-4 WG646909-5 QC Sample: L1320693-04 Client ID: MW- 7D 4 20 238 20 100 0.2 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1320693 10/30/13 Qual Q Qual Qual Serial_No:10301320:59 Page 65 of 77 Nitrogen, Nitrate Chloride Solids, Total Dissolved Solids, Total Dissolved Chemical Oxygen Demand Sulfate Alkalinity, Total 1.05 10 630 260 89 98 221 1.04 9.9 620 270 91. 100 222. mg/l mg/l mg/l mg/l mg/l mg/l mg CaCO3/L 1 1 2 4 2 2 0 17 7 20 20 12 14 10 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG644565-3 QC Sample: L1320740-03 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG644662-3 QC Sample: L1320765-05 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG644982-3 QC Sample: L1320693-01 Client ID: MW-3S General Chemistry - Westborough Lab Associated sample(s): 04-07 QC Batch ID: WG645493-3 QC Sample: L1320765-07 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG645946-4 QC Sample: L1320974-07 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646289-3 QC Sample: L1321297-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-07 QC Batch ID: WG646457-3 QC Sample: L1320693-02 Client ID: MW-3D NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1320693Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 10/30/13 Qual Serial_No:10301320:59 Page 66 of 77 *Values in parentheses indicate holding time in days L1320693-01A L1320693-01B L1320693-01C L1320693-01D L1320693-01E L1320693-01F L1320693-01G L1320693-01H L1320693-02A L1320693-02B L1320693-02C L1320693-02D L1320693-02E L1320693-02F L1320693-02G L1320693-02H L1320693-03A L1320693-03B Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved A A A A A A A A A A A A A A A A A A N/A N/A N/A <2 8 N/A <2 >12 N/A N/A N/A <2 8 N/A <2 >12 N/A N/A 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A Absent Cooler Custody SealCooler Information NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) Project Name: Project Number: L1320693Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/30/13 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:10301320:59 Page 67 of 77 *Values in parentheses indicate holding time in days L1320693-03C L1320693-03D L1320693-03E L1320693-03F L1320693-03G L1320693-03H L1320693-04A L1320693-04B L1320693-04C L1320693-04D L1320693-04E L1320693-04F L1320693-04G L1320693-04H L1320693-05A L1320693-05B L1320693-05C L1320693-05D L1320693-05E L1320693-05F L1320693-05G L1320693-05H L1320693-06A Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved A A A A A A A A A A A A A A A A A A A A A A A N/A <2 8 N/A <2 >12 N/A N/A N/A <2 8 N/A <2 >12 N/A N/A N/A <2 8 N/A <2 >12 N/A 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) Project Name: Project Number: L1320693Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/30/13 Serial_No:10301320:59 Page 68 of 77 *Values in parentheses indicate holding time in days L1320693-06B L1320693-06C L1320693-06D L1320693-06E L1320693-06F L1320693-06G L1320693-06H L1320693-06I L1320693-07A L1320693-07B L1320693-07C L1320693-07D L1320693-07E L1320693-07F L1320693-07G L1320693-07H L1320693-08A Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Plastic 500ml HNO3 preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved A A A A A A A A A A A A A A A A A N/A N/A <2 8 N/A <2 >12 <2 N/A N/A N/A <2 8 N/A <2 >12 N/A 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 5.2 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) CU-6020S(180),FE-SI(180),BA- SI(180),AS-SI(180),MN- SI(180),NA-SI(180),PB- 6020S(180),AG-6020S(180),CR- SI(180),CA-SI(180),CD- 6020S(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) HARDT(180) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) Project Name: Project Number: L1320693Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/30/13 Serial_No:10301320:59 Page 69 of 77 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1320693NANTUCKET LF 1910-97168-CG.SAMP 10/30/13 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G H I - - - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The lower value for the two columns has been reported due to obvious interference. 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:10301320:59 Page 70 of 77 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1320693NANTUCKET LF 1910-97168-CG.SAMP 10/30/13 Data Qualifiers M NJ P Q R RE S - - - - - - - Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. Analytical results are from modified screening analysis. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:10301320:59 Page 71 of 77 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1320693NANTUCKET LF 1910-97168-CG.SAMP REFERENCES 10/30/13 Serial_No:10301320:59 Page 72 of 77 Certificate/Approval Program Summary Last revised October 1, 2013 - Westboro Facility The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative. Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4- Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O- Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) State of Illinois Certificate/Lab ID: 003155. NELAP Accredited. Drinking Water (Inorganic Parameters: SM2120B, 2320B, 2510B, 2540C, SM4500CN-CE, 4500F-C, 4500H-B, 4500NO3-F, 5310C, EPA 200.7, 200.8, 245.1, 300.0. Organic Parameters: EPA 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: SM2120B, 2310B, 2320B, 2340B, 2510B, 2540B, 2540C, 2540D, SM4500CL-E, 4500CN-E, 4500F-C, 4500H-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500P-E, 4500S-D, 4500SO3-B, 5210B, 5220D, 5310C, 5540C, EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1. Organic Parameters: EPA 608, 624, 625.) Hazardous and Solid Waste (Inorganic Parameters: EPA 1010A, 1030, 1311, 1312, 6010C, 6020A, 7196A, 7470A, 7471B, 9012B, 9014, 9038, 9040C, 9045D, 9050A, 9065, 9251. Organic Parameters: 8011 (NPW only), 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8315A, 8330.) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2120B, 2130B, 2320B, 2510C, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, 5310C, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 8315A, 9010C, SM2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-C, 4500NH3-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500P-B, 4500P-E, 4500S2-D, 4500SO3-B, 5540C, 5210B, 5220D, 5310C, 9010B, 9030B, 9040C, 7470A, 7196A, 2340B, EPA 200.7, 6010C, 200.8, 6020A, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8011, 8081B, 8082A, 8330, 8151A, 8260C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Serial_No:10301320:59 Page 73 of 77 Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9040B, 9045C, 6010C, 6020A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B, 9038, 9251. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA- VPH, 8260C, 8270D, 8330, 8151A, 8081B, 8082A, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2- Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW- 846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Hampshire Department of Environmental Services Certificate/Lab ID: 2064. NELAP Accredited. Drinking Water (Organic Parameters: EPA 524.2: Di-isopropyl ether (DIPE), Ethyl-t-butyl ether (ETBE), Tert-amyl methyl ether (TAME)). Non-Potable Water (Organic Parameters: EPA 8260C: 1,3,5-Trichlorobenzene. EPA 8015C(M): TPH.) Solid & Chemical Materials (Organic Parameters: EPA 8260C: 1,3,5-Trichlorobenzene.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310C, 4500-PE, EPA 420.1, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, 4500SO4-E, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 5030C, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, Serial_No:10301320:59 Page 74 of 77 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5030C, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.1, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2340B, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010C, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 8315A, 3005A, 9010C, 9030B. Organic Parameters: EPA 624, 8260C, 8270D, 8270D-SIM, 625, 608, 8081B, 8151A, 8330A, 8082A, EPA 3510C, 5030B, 5030C, 8015C, 8011.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010C, 6020A, 7196A, 7471B, 8315A, 9012B, 9014, 9065, 9050A, 9038, 9251, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260C, 8270D, 8270D-SIM, 8015C, 8081B, 8151A, 8330A, 8082A, 3540C, 3546, 3580A, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9012B, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F- C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D- SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL- E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.1, 2320B, 4500F-C, 4500NO3-F, 4500H+B, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 350.1, 351.1, 351.2, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 2340B, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204- 00-1-X, 7196A, 7470A, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, Serial_No:10301320:59 Page 75 of 77 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500 SO3-B, 4500H-B, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C, 9010Cm 9030B, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9010C, 9012B, 9030B, 9014, 9038, 9040C, 9045D, 9251, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 3550B, 3580A, 3620C, 3630C, 6020A, 8260B, 8260C, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010C, 6020A, 245.1, 7470A, 9040B, 9010B, 180.1, 300.0, 332.0, 6860, 351.1, 353.2, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500Norg-C, 4500NO3-F, 5310C, 2130B, 2320B, 2340B, 2540C, 5540C, 3005A, 3015, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8015C, 8151A, 8260C, 8270D, 8270D-SIM, 8330A, 8082A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010C, 6020A, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9040B, 9045C, 9010C, 9012B, 9251, SM3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8015C, 8151A, 8260C, 8270D, 8270D-SIM, 8330A/B-prep, 8082A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone (MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5- Trichlorobenzene, 4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260B: 1,2,4,5- Tetramethylbenzene, 4-Ethyltoluene. EPA 8260 Non-potable water matrix: Iodomethane (methyl iodide), Methyl methacrylate. EPA 8260 Soil matrix: Tert-amyl methyl ether (TAME), Diisopropyl ether (DIPE), Azobenzene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Serial_No:10301320:59 Page 76 of 77 Serial_No:10301320:59 Page 77 of 77 L1320833 CDM Smith, Inc. 1910-97168-CG.SAMP NANTUCKET LANDFILL Client: Project Name: Project Number: 10/31/13 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:10311315:59 Page 1 of 79 L1320833-01 L1320833-02 L1320833-03 L1320833-04 L1320833-05 L1320833-06 L1320833-07 L1320833-08 L1320833-09 Alpha Sample ID MW-8S MW-8D MW-1S MW-1D MW-6S MW-6D MW-5S MW-5D TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LANDFILL 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320833 10/31/13 10/16/13 09:00 10/16/13 09:30 10/16/13 10:30 10/16/13 11:30 10/16/13 12:15 10/16/13 12:50 10/16/13 14:25 10/16/13 15:00 10/16/13 00:00 Collection Date/Time Serial_No:10311315:59 Page 2 of 79 NANTUCKET LANDFILL 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320833 10/31/13 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed. Please contact Client Services at 800-624-9220 with any questions. Serial_No:10311315:59 Page 3 of 79 Case Narrative (continued) NANTUCKET LANDFILL 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1320833 10/31/13 Sample Receipt L1320833-01 through -08 were field filtered for Dissolved Metals. Sulfate L1320833-01 has an elevated detection limit due to the dilution required by the sample matrix. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 10/31/13 Serial_No:10311315:59 Page 4 of 79 ORGANICS Serial_No:10311315:59 Page 5 of 79 VOLATILES Serial_No:10311315:59 Page 6 of 79 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-8SClient ID: 10/16/13 09:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 14:07 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 7 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-8SClient ID: 10/16/13 09:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 8 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 100 95 105 94 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-8SClient ID: 10/16/13 09:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 9 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-8DClient ID: 10/16/13 09:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 14:43 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 10 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-8DClient ID: 10/16/13 09:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 11 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 98 94 100 94 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-8DClient ID: 10/16/13 09:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 12 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-1SClient ID: 10/16/13 10:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 15:19 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 13 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-1SClient ID: 10/16/13 10:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 14 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 101 94 101 95 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-1SClient ID: 10/16/13 10:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 15 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-1DClient ID: 10/16/13 11:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 15:55 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 16 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-1DClient ID: 10/16/13 11:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 17 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 102 94 97 95 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-1DClient ID: 10/16/13 11:30Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 18 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-6SClient ID: 10/16/13 12:15Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 16:31 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 19 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-6SClient ID: 10/16/13 12:15Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 20 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 102 94 102 95 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-6SClient ID: 10/16/13 12:15Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 21 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-6DClient ID: 10/16/13 12:50Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 17:07 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 22 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-6DClient ID: 10/16/13 12:50Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 23 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 103 93 103 96 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-6DClient ID: 10/16/13 12:50Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 24 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-5SClient ID: 10/16/13 14:25Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 17:43 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 25 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-5SClient ID: 10/16/13 14:25Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 26 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 103 94 102 96 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-5SClient ID: 10/16/13 14:25Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 27 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 MW-5DClient ID: 10/16/13 15:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-08Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 18:19 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 28 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 MW-5DClient ID: 10/16/13 15:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 29 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 104 94 99 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 MW-5DClient ID: 10/16/13 15:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:10311315:59 Page 30 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 10/31/13 TRIP BLANKClient ID: 10/16/13 00:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-09Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 10/21/13 18:55 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 31 of 79 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 10/31/13 TRIP BLANKClient ID: 10/16/13 00:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 32 of 79 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 104 95 106 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 10/31/13 TRIP BLANKClient ID: 10/16/13 00:00Date Collected: 10/17/13Date Received: NANTUCKET, MASample Location: L1320833-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- Serial_No:10311315:59 Page 33 of 79 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/21/13 11:02 1,8260CAnalytical Method: Analytical Date: 10/31/13 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG645653-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 34 of 79 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/21/13 11:02 1,8260CAnalytical Method: Analytical Date: 10/31/13 Analyst:PD Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG645653-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 35 of 79 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/21/13 11:02 1,8260CAnalytical Method: Analytical Date: 10/31/13 Analyst:PD Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND RL 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG645653-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 98 95 105 95 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 36 of 79 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 110 105 108 107 101 107 104 106 105 111 109 106 109 107 105 104 111 103 103 102 105 109 103 106 105 103 108 106 103 104 109 109 105 108 107 104 103 116 109 103 102 104 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 1 2 2 2 2 1 2 3 1 2 0 1 1 0 1 1 4 6 0 0 1 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG645653-1 WG645653-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 37 of 79 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 133 134 105 107 101 104 104 108 106 105 103 107 107 105 106 99 102 109 95 146 105 133 143 108 108 101 101 102 108 107 104 103 104 105 103 105 105 108 108 92 104 100 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 0 6 3 1 0 3 2 0 1 1 0 3 2 2 1 6 6 1 3 34 5 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG645653-1 WG645653-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Q Q Q Qual Q Serial_No:10311315:59 Page 38 of 79 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 133 101 103 119 100 104 110 104 111 105 103 109 105 108 107 105 106 105 101 112 104 120 103 110 112 104 105 111 102 107 104 105 109 107 98 102 102 106 104 108 104 106 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 10 2 7 6 4 1 1 2 4 1 2 0 2 10 5 3 0 1 7 7 2 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG645653-1 WG645653-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 39 of 79 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 108 126 104 120 116 109 108 105 102 101 101 116 102 105 104 104 102 110 105 105 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 7 8 2 13 11 5 6 5 3 4 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG645653-1 WG645653-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 98 95 92 96 70-130 70-130 70-130 70-130 99 94 95 96 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 10/31/13 Acceptance Criteria Qual Qual Qual Serial_No:10311315:59 Page 40 of 79 METALS Serial_No:10311315:59 Page 41 of 79 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-8SClient ID: 10/16/13 09:00Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 0.0143 0.0209 ND 30. ND ND 5.1 ND 0.375 ND ND ND 40. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/29/13 17:23 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 10/31/13 13:25 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 42 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-8DClient ID: 10/16/13 09:30Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 1.9 ND ND ND ND ND ND ND ND 11. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/29/13 17:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 10/31/13 13:29 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 43 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-1SClient ID: 10/16/13 10:30Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 1.8 ND ND ND ND ND ND ND ND 16. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/29/13 17:35 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 10/31/13 13:33 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 44 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-1DClient ID: 10/16/13 11:30Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 16. ND ND ND ND ND ND ND ND 12. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/29/13 17:37 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 10/31/13 13:36 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 45 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-6SClient ID: 10/16/13 12:15Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0881 ND 13. ND ND ND ND 0.269 ND ND ND 23. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/29/13 17:39 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 10/31/13 13:40 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 46 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-6DClient ID: 10/16/13 12:50Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 3.5 ND ND ND ND ND ND ND ND 16. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/29/13 17:40 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 10/31/13 13:44 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 47 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-5SClient ID: 10/16/13 14:25Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0373 ND 1.7 ND ND 1.3 ND 0.236 ND ND ND 23. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/29/13 17:42 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 10/31/13 13:48 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 48 of 79 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 SAMPLE RESULTS MW-5DClient ID: 10/16/13 15:00Date Collected: 10/17/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1320833-08Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 7.3 ND ND ND ND 0.598 ND ND ND 45. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/29/13 17:44 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 10/31/13 12:50 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL DR KL KL KL KL 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 49 of 79 FF Parameter Parameter Result Result Dilution Factor Dilution Factor Qualifier Qualifier Units Units RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Date Analyzed Date Analyzed Analytical Method Analytical Method Analyst Analyst Date Prepared Date Prepared 10/31/13 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.00020 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 10/29/13 17:20 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 10/31/13 12:42 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C DR KL KL KL KL KL KL KL KL KL KL KL KL KL 10/29/13 09:30 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 10/20/13 09:48 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG647706-1 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG648041-1 EPA 7470A NA Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:10311315:59 Page 50 of 79 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 102 102 101 100 100 90 95 100 104 96 108 99 110 100 - - - - - - - - - - - - - - 70-130 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG647706-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG648041-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 51 of 79 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND 7.3 ND ND ND ND 0.598 ND ND 45 ND 0.00599 0.125 1.98 0.0497 17 0.18 0.237 1.0 0.510 1.04 0.130 0.0492 54 0.486 120 104 99 97 97 90 95 100 100 88 108 98 90 97 - - - - - - - - - - - - - - - - - - - - - - - - - - - - 70-130 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647706-4 QC Sample: L1320833-01 Client ID: MW-8S Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG648041-4 QC Sample: L1320833-08 Client ID: MW-5D 0.005 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 52 of 79 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND 7.3 ND ND ND ND 0.598 ND ND 45 ND ND ND ND ND 7.3 ND ND ND ND 0.597 ND ND 45. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l NC NC NC NC 0 NC NC NC NC 0 NC NC 0 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647706-3 QC Sample: L1320833-01 Client ID: MW-8S Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG648041-3 QC Sample: L1320833-08 Client ID: MW-5D NANTUCKET LANDFILL 1910-97168-CG.SA Project Name: Project Number: L1320833Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 10/31/13 Qual Serial_No:10311315:59 Page 53 of 79 INORGANICS & MISCELLANEOUS Serial_No:10311315:59 Page 54 of 79 FF MW-8SClient ID: 10/16/13 09:00Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 128. 290 ND 49. ND ND 80. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:15 10/21/13 18:10 10/18/13 03:30 10/25/13 16:45 10/25/13 20:00 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 55 of 79 FF MW-8DClient ID: 10/16/13 09:30Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 6.40 40. ND 17. 0.704 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:16 10/21/13 18:11 10/18/13 02:36 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 56 of 79 FF MW-1SClient ID: 10/16/13 10:30Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 3.70 53. ND 29. ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:17 10/21/13 18:11 10/18/13 02:36 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 57 of 79 FF MW-1DClient ID: 10/16/13 11:30Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 44.9 86. ND 16. 0.273 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:19 10/21/13 18:15 10/18/13 02:37 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 58 of 79 FF MW-6SClient ID: 10/16/13 12:15Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 6.20 120 ND 43. 6.47 16. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:20 10/21/13 18:16 10/18/13 02:38 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 59 of 79 FF MW-6DClient ID: 10/16/13 12:50Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 7.60 70. ND 25. 1.09 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:21 10/21/13 18:17 10/18/13 02:40 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 60 of 79 FF MW-5SClient ID: 10/16/13 14:25Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand ND 89. ND 37. 0.204 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 14:21 10/21/13 18:18 10/18/13 02:41 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/25/13 11:00 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 61 of 79 FF MW-5DClient ID: 10/16/13 15:00Date Collected: 10/17/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1320833-08Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 25.2 180 ND 63. ND 16. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 10/27/13 17:59 10/22/13 13:15 10/28/13 15:01 10/21/13 18:19 10/18/13 02:42 10/25/13 16:45 10/25/13 20:01 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SP DW JO LA DB MP TL Date Prepared - - 10/27/13 17:50 - - 10/25/13 16:45 10/25/13 16:35 10/31/13 MDL NA -- -- -- -- -- -- Serial_No:10311315:59 Page 62 of 79 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 Date Analyzed Analytical Method Analyst Date Prepared 10/31/13 Nitrogen, Nitrate Chloride Solids, Total Dissolved Sulfate Cyanide, Total Cyanide, Total Chemical Oxygen Demand Cyanide, Total Alkalinity, Total ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg CaCO3/L 1 1 1 1 1 1 1 1 1 0.100 1.0 10 10 0.005 0.005 20 0.005 2.00 10/18/13 01:48 10/21/13 17:53 10/22/13 13:15 10/25/13 16:45 10/28/13 14:10 10/28/13 14:10 10/25/13 19:59 10/28/13 14:48 10/27/13 17:59 30,4500NO3-F 1,9251 30,2540C 1,9038 1,9010C/9012A 1,9010C/9012A 30,5220D 1,9010C/9012A 30,2320B DB LA DW MP JO JO TL JO SP - - - 10/25/13 16:45 10/25/13 11:00 10/25/13 11:00 10/25/13 16:35 10/27/13 17:50 - General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG644917-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG645662-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG645808-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG646989-1 General Chemistry - Westborough Lab for sample(s): 01-03 Batch: WG647016-1 General Chemistry - Westborough Lab for sample(s): 04-07 Batch: WG647040-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG647105-1 General Chemistry - Westborough Lab for sample(s): 08 Batch: WG647372-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG647374-1 MDL -- -- -- -- -- -- -- -- NA Serial_No:10311315:59 Page 63 of 79 Nitrogen, Nitrate Chloride Solids, Total Dissolved Sulfate Cyanide, Total Cyanide, Total Chemical Oxygen Demand 105 97 97 90 103 104 98 - - - - 103 103 - 90-110 90-110 80-120 84-119 80-120 80-120 93-106 - - - - 0 1 - 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG644917-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG645662-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG645808-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG646989-2 General Chemistry - Westborough Lab Associated sample(s): 01-03 Batch: WG647016-2 WG647016-3 General Chemistry - Westborough Lab Associated sample(s): 04-07 Batch: WG647040-2 WG647040-3 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG647105-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 64 of 79 Cyanide, Total Alkalinity, Total 108 106 102 - 80-120 90-110 6 - 20 10 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 08 Batch: WG647372-4 WG647372-5 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG647374-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Serial_No:10311315:59 Page 65 of 79 Nitrogen, Nitrate Chloride Sulfate Cyanide, Total Cyanide, Total Chemical Oxygen Demand Cyanide, Total Alkalinity, Total ND 120 ND ND ND ND ND 18.8 3.93 130 24 0.204 0.205 260 0.203 124 98 79 120 102 102 107 102 105 - - - 0.202 0.204 - 0.203 - - - - 101 102 - 102 - 83-113 58-140 55-147 80-120 80-120 84-120 80-120 86-116 - - - 1 0 - 0 - 17 7 14 20 20 12 20 10 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG644917-4 QC Sample: L1320833-01 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG645662-4 QC Sample: L1321033-02 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG646989-4 QC Sample: L1320833-03 Client ID: MW-1S General Chemistry - Westborough Lab Associated sample(s): 01-03 QC Batch ID: WG647016-4 WG647016-5 QC Sample: L1321393-05 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 04-07 QC Batch ID: WG647040-4 WG647040-5 QC Sample: L1320833-07 Client ID: MW- 5S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647105-3 QC Sample: L1321393-01 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 08 QC Batch ID: WG647372-3 WG647372-2 QC Sample: L1320833-08 Client ID: MW-5D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647374-4 QC Sample: L1320600-02 Client ID: MS Sample 4 20 20 0.2 0.2 238 0.2 100 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-97168-CG.SAMP L1320833 10/31/13 Qual Qual Qual Serial_No:10311315:59 Page 66 of 79 Nitrogen, Nitrate Chloride Solids, Total Dissolved Sulfate Chemical Oxygen Demand Alkalinity, Total ND 120 290 ND ND 28.2 ND 110 320 ND ND 28.1 mg/l mg/l mg/l mg/l mg/l mg CaCO3/L NC 9 10 NC NC 0 17 7 20 14 12 10 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG644917-3 QC Sample: L1320833-01 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG645662-3 QC Sample: L1321033-02 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG645808-3 QC Sample: L1320833-01 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG646989-3 QC Sample: L1320833-02 Client ID: MW-8D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647105-4 QC Sample: L1321393-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG647374-3 QC Sample: L1320600-01 Client ID: DUP Sample NANTUCKET LANDFILL 1910-97168-CG.SA Project Name: Project Number: L1320833Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 10/31/13 Qual Q Serial_No:10311315:59 Page 67 of 79 *Values in parentheses indicate holding time in days L1320833-01A L1320833-01D L1320833-01E L1320833-01F L1320833-01G L1320833-01H L1320833-02A L1320833-02B L1320833-02C L1320833-02D L1320833-02E L1320833-02F L1320833-02G L1320833-02H L1320833-03A L1320833-03B L1320833-03C Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved A A A A A A A A A A A A A A A A A N/A <2 7 N/A <2 >12 N/A N/A N/A <2 7 N/A <2 >12 N/A N/A N/A 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A B Absent Absent Cooler Custody SealCooler Information NANTUCKET LANDFILL 1910-97168-CG.SAMP 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) Project Name: Project Number: L1320833Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/31/13 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:10311315:59 Page 68 of 79 *Values in parentheses indicate holding time in days L1320833-03D L1320833-03E L1320833-03F L1320833-03G L1320833-03H L1320833-04A L1320833-04B L1320833-04C L1320833-04D L1320833-04E L1320833-04F L1320833-04G L1320833-04H L1320833-05A L1320833-05B L1320833-05C L1320833-05D L1320833-05E L1320833-05F L1320833-05G L1320833-05H L1320833-06A L1320833-06B Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved A A A A A A A A A A A A A B B B B B B B B B B <2 7 N/A <2 >12 N/A N/A N/A <2 7 N/A <2 >12 N/A N/A N/A <2 7 N/A <2 >12 N/A N/A 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.8 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LANDFILL 1910-97168-CG.SAMP COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) Project Name: Project Number: L1320833Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/31/13 Serial_No:10311315:59 Page 69 of 79 *Values in parentheses indicate holding time in days L1320833-06C L1320833-06D L1320833-06E L1320833-06F L1320833-06G L1320833-06H L1320833-07A L1320833-07B L1320833-07C L1320833-07D L1320833-07E L1320833-07F L1320833-07G L1320833-07H L1320833-08A L1320833-08B L1320833-08C L1320833-08D L1320833-08E L1320833-08F L1320833-08G L1320833-08H L1320833-09A Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 500ml unpreserved Plastic 250ml unpreserved Plastic 250ml HNO3 preserved Plastic 250ml NaOH preserved Vial HCl preserved B B B B B B B B B B B B B B B B B B B B B B B N/A <2 7 N/A <2 >12 N/A N/A N/A <2 7 N/A <2 >12 N/A N/A N/A <2 7 N/A <2 >12 N/A 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LANDFILL 1910-97168-CG.SAMP 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) 8260(14) 8260(14) COD-5220(28) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) TCN-9010(14) 8260(14) Project Name: Project Number: L1320833Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/31/13 Serial_No:10311315:59 Page 70 of 79 *Values in parentheses indicate holding time in days L1320833-09B Vial HCl preserved B N/A 5.0 Y Absent NANTUCKET LANDFILL 1910-97168-CG.SAMP 8260(14) Project Name: Project Number: L1320833Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 10/31/13 Serial_No:10311315:59 Page 71 of 79 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1320833NANTUCKET LANDFILL 1910-97168-CG.SAMP 10/31/13 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G H I - - - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The lower value for the two columns has been reported due to obvious interference. 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:10311315:59 Page 72 of 79 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1320833NANTUCKET LANDFILL 1910-97168-CG.SAMP 10/31/13 Data Qualifiers M NJ P Q R RE S - - - - - - - Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. Analytical results are from modified screening analysis. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:10311315:59 Page 73 of 79 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IV, 2007. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1320833NANTUCKET LANDFILL 1910-97168-CG.SAMP REFERENCES 10/31/13 Serial_No:10311315:59 Page 74 of 79 Certificate/Approval Program Summary Last revised October 1, 2013 - Westboro Facility The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative. Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4- Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O- Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) State of Illinois Certificate/Lab ID: 003155. NELAP Accredited. Drinking Water (Inorganic Parameters: SM2120B, 2320B, 2510B, 2540C, SM4500CN-CE, 4500F-C, 4500H-B, 4500NO3-F, 5310C, EPA 200.7, 200.8, 245.1, 300.0. Organic Parameters: EPA 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: SM2120B, 2310B, 2320B, 2340B, 2510B, 2540B, 2540C, 2540D, SM4500CL-E, 4500CN-E, 4500F-C, 4500H-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500P-E, 4500S-D, 4500SO3-B, 5210B, 5220D, 5310C, 5540C, EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1. Organic Parameters: EPA 608, 624, 625.) Hazardous and Solid Waste (Inorganic Parameters: EPA 1010A, 1030, 1311, 1312, 6010C, 6020A, 7196A, 7470A, 7471B, 9012B, 9014, 9038, 9040C, 9045D, 9050A, 9065, 9251. Organic Parameters: 8011 (NPW only), 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8315A, 8330.) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2120B, 2130B, 2320B, 2510C, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, 5310C, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 8315A, 9010C, SM2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-C, 4500NH3-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500P-B, 4500P-E, 4500S2-D, 4500SO3-B, 5540C, 5210B, 5220D, 5310C, 9010B, 9030B, 9040C, 7470A, 7196A, 2340B, EPA 200.7, 6010C, 200.8, 6020A, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8011, 8081B, 8082A, 8330, 8151A, 8260C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Serial_No:10311315:59 Page 75 of 79 Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9040B, 9045C, 6010C, 6020A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B, 9038, 9251. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA- VPH, 8260C, 8270D, 8330, 8151A, 8081B, 8082A, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2- Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW- 846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Hampshire Department of Environmental Services Certificate/Lab ID: 2064. NELAP Accredited. Drinking Water (Organic Parameters: EPA 524.2: Di-isopropyl ether (DIPE), Ethyl-t-butyl ether (ETBE), Tert-amyl methyl ether (TAME)). Non-Potable Water (Organic Parameters: EPA 8260C: 1,3,5-Trichlorobenzene. EPA 8015C(M): TPH.) Solid & Chemical Materials (Organic Parameters: EPA 8260C: 1,3,5-Trichlorobenzene.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310C, 4500-PE, EPA 420.1, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, 4500SO4-E, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 5030C, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, Serial_No:10311315:59 Page 76 of 79 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5030C, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.1, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2340B, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010C, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 8315A, 3005A, 9010C, 9030B. Organic Parameters: EPA 624, 8260C, 8270D, 8270D-SIM, 625, 608, 8081B, 8151A, 8330A, 8082A, EPA 3510C, 5030B, 5030C, 8015C, 8011.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010C, 6020A, 7196A, 7471B, 8315A, 9012B, 9014, 9065, 9050A, 9038, 9251, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260C, 8270D, 8270D-SIM, 8015C, 8081B, 8151A, 8330A, 8082A, 3540C, 3546, 3580A, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9012B, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F- C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D- SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL- E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.1, 2320B, 4500F-C, 4500NO3-F, 4500H+B, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 350.1, 351.1, 351.2, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 2340B, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204- 00-1-X, 7196A, 7470A, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, Serial_No:10311315:59 Page 77 of 79 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500 SO3-B, 4500H-B, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C, 9010Cm 9030B, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9010C, 9012B, 9030B, 9014, 9038, 9040C, 9045D, 9251, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 3550B, 3580A, 3620C, 3630C, 6020A, 8260B, 8260C, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010C, 6020A, 245.1, 7470A, 9040B, 9010B, 180.1, 300.0, 332.0, 6860, 351.1, 353.2, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500Norg-C, 4500NO3-F, 5310C, 2130B, 2320B, 2340B, 2540C, 5540C, 3005A, 3015, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8015C, 8151A, 8260C, 8270D, 8270D-SIM, 8330A, 8082A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010C, 6020A, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9040B, 9045C, 9010C, 9012B, 9251, SM3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8015C, 8151A, 8260C, 8270D, 8270D-SIM, 8330A/B-prep, 8082A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 524.2: Acetone, 2-Butanone (Methyl ethyl ketone (MEK)), Tert-butyl alcohol, 2-Hexanone, Tetrahydrofuran, 1,3,5- Trichlorobenzene, 4-Methyl-2-pentanone (MIBK), Carbon disulfide, Diethyl ether. EPA 8260B: 1,2,4,5- Tetramethylbenzene, 4-Ethyltoluene. EPA 8260 Non-potable water matrix: Iodomethane (methyl iodide), Methyl methacrylate. EPA 8260 Soil matrix: Tert-amyl methyl ether (TAME), Diisopropyl ether (DIPE), Azobenzene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine. EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Serial_No:10311315:59 Page 78 of 79 Serial_No:10311315:59 Page 79 of 79