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HomeMy WebLinkAbout2013-03 Nantucket Landfill - Semi-Annual Environmental Monitoring Report REPORT Summary of Groundwater, Surface Water, and Landfill Gas Sampling Results Nantucket Landfill Nantucket, Massachusetts March 2013 Appendix A Site Plan Appendix B Sampling Results Summary Tables Appendix C Laboratory Reports and Chains of Custody L1304142 CDM Smith, Inc. 1910-88908-CG.SAMP NANTUCKET LANDFILL Client: Project Name: Project Number: 03/20/13 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:03201317:51 Page 1 of 78 L1304142-01 L1304142-02 L1304142-03 L1304142-04 L1304142-05 L1304142-06 L1304142-07 L1304142-08 L1304142-09 Alpha Sample ID MW-5S MW-5D MW-6S MW-6D MW-1S MW-1D MW-8S MW-8D TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LANDFILL 1910-88908-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304142 03/20/13 03/12/13 08:40 03/12/13 09:00 03/12/13 09:45 03/12/13 10:30 03/12/13 11:00 03/12/13 11:45 03/12/13 13:05 03/12/13 14:00 03/12/13 00:00 Collection Date/Time Serial_No:03201317:51 Page 2 of 78 NANTUCKET LANDFILL 1910-88908-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304142 03/20/13 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30 days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Please contact Client Services at 800-624-9220 with any questions. Serial_No:03201317:51 Page 3 of 78 Case Narrative (continued) NANTUCKET LANDFILL 1910-88908-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304142 03/20/13 Sample Receipt L1304142-05 and -07 were received below the appropriate pH for the Cyanide analysis. The laboratory added additional NaOH to a pH >12. The samples were field filtered for Dissolved Metals. Chloride The WG595209-4 MS recovery (50%), performed on L1304142-02, is outside the acceptance criteria; however, the associated LCS recovery is within overall method allowances. No further action was required. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 03/20/13 Serial_No:03201317:51 Page 4 of 78 ORGANICS Serial_No:03201317:51 Page 5 of 78 VOLATILES Serial_No:03201317:51 Page 6 of 78 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-5SClient ID: 03/12/13 08:40Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 14:31 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 7 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-5SClient ID: 03/12/13 08:40Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 8 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 125 102 117 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-5SClient ID: 03/12/13 08:40Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 9 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-5DClient ID: 03/12/13 09:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 14:56 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 10 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-5DClient ID: 03/12/13 09:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 11 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 125 105 119 95 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-5DClient ID: 03/12/13 09:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 12 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-6SClient ID: 03/12/13 09:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 15:22 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 13 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-6SClient ID: 03/12/13 09:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 14 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 125 104 118 96 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-6SClient ID: 03/12/13 09:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 15 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-6DClient ID: 03/12/13 10:30Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 15:47 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 16 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-6DClient ID: 03/12/13 10:30Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 17 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 123 104 118 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-6DClient ID: 03/12/13 10:30Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 18 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-1SClient ID: 03/12/13 11:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 16:12 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 19 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-1SClient ID: 03/12/13 11:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 20 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 122 104 118 95 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-1SClient ID: 03/12/13 11:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 21 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-1DClient ID: 03/12/13 11:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 16:38 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 22 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-1DClient ID: 03/12/13 11:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 23 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 124 104 116 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-1DClient ID: 03/12/13 11:45Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 24 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-8SClient ID: 03/12/13 13:05Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 17:03 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 25 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND 9.6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-8SClient ID: 03/12/13 13:05Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 26 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 129 103 116 98 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-8SClient ID: 03/12/13 13:05Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 27 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 MW-8DClient ID: 03/12/13 14:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-08Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 17:28 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 28 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 MW-8DClient ID: 03/12/13 14:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 29 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 124 104 118 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 MW-8DClient ID: 03/12/13 14:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03201317:51 Page 30 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/20/13 TRIP BLANKClient ID: 03/12/13 00:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-09Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/14/13 17:54 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 31 of 78 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/20/13 TRIP BLANKClient ID: 03/12/13 00:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 32 of 78 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 129 103 116 98 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/20/13 TRIP BLANKClient ID: 03/12/13 00:00Date Collected: 03/13/13Date Received: NANTUCKET, MASample Location: L1304142-09Lab ID: Field Prep:Not Specified MDL -- -- -- -- Serial_No:03201317:51 Page 33 of 78 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/14/13 09:53 1,8260CAnalytical Method: Analytical Date: 03/20/13 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG595478-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 34 of 78 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/14/13 09:53 1,8260CAnalytical Method: Analytical Date: 03/20/13 Analyst:PD Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG595478-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 35 of 78 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/14/13 09:53 1,8260CAnalytical Method: Analytical Date: 03/20/13 Analyst:PD Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND RL 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-09 Batch: WG595478-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 123 103 115 96 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 36 of 78 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 106 116 109 95 117 95 110 85 97 92 126 102 109 112 109 108 87 118 106 103 106 109 122 116 101 120 97 114 90 101 98 128 107 111 114 113 113 91 120 111 108 110 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 3 5 6 6 3 2 4 6 4 6 2 5 2 2 4 5 4 2 5 5 4 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG595478-1 WG595478-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Qual Serial_No:03201317:51 Page 37 of 78 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 117 82 100 107 95 97 100 98 97 97 114 101 102 98 105 138 96 104 97 138 100 101 74 104 112 102 103 105 101 101 100 117 106 106 103 107 140 97 107 104 151 106 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 15 10 4 5 7 6 5 3 4 3 3 5 4 5 2 1 1 3 7 9 6 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG595478-1 WG595478-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Q Q Q Qual Serial_No:03201317:51 Page 38 of 78 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 129 138 118 139 107 127 92 124 110 102 115 94 95 114 108 103 105 114 122 84 107 142 139 116 150 111 133 97 129 116 104 116 98 98 118 112 108 116 119 124 85 112 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 10 1 2 8 4 5 5 4 5 2 1 4 3 3 4 5 10 4 2 1 5 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG595478-1 WG595478-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Q Q Q Q Q Q Qual Serial_No:03201317:51 Page 39 of 78 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 104 102 112 90 91 108 109 116 103 117 107 102 118 90 92 111 113 114 108 116 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 3 0 5 0 1 3 4 2 5 1 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-09 Batch: WG595478-1 WG595478-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 121 104 115 97 70-130 70-130 70-130 70-130 121 104 114 98 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 03/20/13 Acceptance Criteria Qual Qual Qual Serial_No:03201317:51 Page 40 of 78 METALS Serial_No:03201317:51 Page 41 of 78 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-5SClient ID: 03/12/13 08:40Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0287 ND 5.3 ND ND 0.60 ND 0.265 ND ND ND 20. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/15/13 10:23 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 03/19/13 14:57 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 42 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-5DClient ID: 03/12/13 09:00Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0284 ND 13. ND ND ND ND 0.771 ND ND ND 240 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/15/13 10:25 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 03/19/13 15:08 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 43 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-6SClient ID: 03/12/13 09:45Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0504 ND 24. ND ND 0.064 ND 0.0291 ND ND ND 51. 0.114 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/15/13 10:27 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 03/19/13 15:12 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 44 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-6DClient ID: 03/12/13 10:30Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 3.7 ND ND ND ND ND ND ND ND 15. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/15/13 10:29 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 03/19/13 15:16 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 45 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-1SClient ID: 03/12/13 11:00Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 3.2 ND ND ND ND ND ND ND ND 13. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/15/13 10:31 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 03/19/13 15:20 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 46 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-1DClient ID: 03/12/13 11:45Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 16. ND ND ND ND ND ND ND ND 10. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/15/13 10:33 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 03/19/13 15:24 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 47 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-8SClient ID: 03/12/13 13:05Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0634 ND 99. ND 0.0428 0.74 ND 0.694 ND ND ND 91. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/15/13 10:38 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 03/19/13 15:28 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 48 of 78 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 SAMPLE RESULTS MW-8DClient ID: 03/12/13 14:00Date Collected: 03/13/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304142-08Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND 5.0 ND ND ND ND 0.160 ND ND ND 11. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/15/13 10:46 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 03/19/13 14:34 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C BM BM BM BM BM BM BM BM BM JH BM BM BM BM 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 49 of 78 FF Parameter Parameter Result Result Dilution Factor Dilution Factor Qualifier Qualifier Units Units RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Date Analyzed Date Analyzed Analytical Method Analytical Method Analyst Analyst Date Prepared Date Prepared 03/20/13 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.00020 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 03/15/13 09:55 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 03/19/13 14:26 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C JH BM BM BM BM BM BM BM BM BM BM BM BM BM 03/14/13 19:41 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 03/18/13 15:40 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG595373-1 Dissolved Metals - Westborough Lab for sample(s): 01-08 Batch: WG595952-1 EPA 7470A NA Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03201317:51 Page 50 of 78 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 82 118 114 118 120 115 108 110 109 109 114 111 110 112 - - - - - - - - - - - - - - 70-130 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG595373-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-08 Batch: WG595952-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Qual Serial_No:03201317:51 Page 51 of 78 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND 5.0 ND ND ND ND 0.160 ND ND 11 ND 0.00101 0.129 2.08 0.0540 15 0.21 0.250 1.0 0.500 0.629 0.124 0.0485 20 0.519 101 108 104 106 100 105 100 100 98 94 103 97 90 104 - - - - - - - - - - - - - - - - - - - - - - - - - - - - 70-130 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595373-4 QC Sample: L1304045-01 Client ID: MS Sample Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595952-4 QC Sample: L1304142-08 Client ID: MW-8D 0.001 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 MS Added Matrix Spike Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Qual Serial_No:03201317:51 Page 52 of 78 Mercury, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND 5.0 ND ND ND ND 0.160 ND ND 11 ND ND ND ND ND 4.8 ND ND ND ND 0.151 ND ND 10. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l NC NC NC NC 4 NC NC NC NC 6 NC NC 10 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595373-3 QC Sample: L1304045-01 Client ID: DUP Sample Dissolved Metals - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595952-3 QC Sample: L1304142-08 Client ID: MW-8D NANTUCKET LANDFILL 1910-88908-CG.SA Project Name: Project Number: L1304142Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 03/20/13 Qual Serial_No:03201317:51 Page 53 of 78 INORGANICS & MISCELLANEOUS Serial_No:03201317:51 Page 54 of 78 FF MW-5SClient ID: 03/12/13 08:40Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 6.30 100 ND 38. 0.157 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:42 03/14/13 11:24 03/13/13 22:36 03/18/13 15:45 03/14/13 21:21 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 55 of 78 FF MW-5DClient ID: 03/12/13 09:00Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 22.8 790 0.013 400 0.148 44. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 10 1 2 1 2.00 10 0.005 10 0.100 20 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:31 03/14/13 11:56 03/13/13 22:09 03/18/13 15:45 03/14/13 21:21 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 56 of 78 FF MW-6SClient ID: 03/12/13 09:45Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 13.2 250 ND 100 1.98 19. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 5 1 1 1 2.00 10 0.005 5.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:33 03/14/13 11:53 03/13/13 22:09 03/18/13 15:45 03/14/13 21:21 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 57 of 78 FF MW-6DClient ID: 03/12/13 10:30Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 7.30 87. ND 28. 1.13 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:34 03/14/13 11:54 03/13/13 22:12 03/18/13 15:45 03/14/13 21:22 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 58 of 78 FF MW-1SClient ID: 03/12/13 11:00Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 7.60 84. ND 24. ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:35 03/14/13 11:33 03/13/13 22:13 03/18/13 15:45 03/14/13 21:22 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 59 of 78 FF MW-1DClient ID: 03/12/13 11:45Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 66.2 100 ND 15. 0.169 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:36 03/14/13 11:34 03/13/13 22:13 03/18/13 15:45 03/14/13 21:22 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 60 of 78 FF MW-8SClient ID: 03/12/13 13:05Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 378. 1000 ND 100 2.29 180 310 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 5 1 10 1 2.00 10 0.005 5.0 0.100 100 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:37 03/14/13 12:02 03/13/13 22:14 03/18/13 15:45 03/14/13 21:22 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 61 of 78 FF MW-8DClient ID: 03/12/13 14:00Date Collected: 03/13/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304142-08Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 17.4 76. ND 17. 0.196 ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/18/13 12:15 03/14/13 15:37 03/14/13 12:03 03/13/13 22:15 03/18/13 15:45 03/14/13 21:22 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW JO LA DB MP TL Date Prepared - - 03/14/13 10:05 - - 03/18/13 15:45 03/14/13 17:30 03/20/13 MDL NA -- -- -- -- -- -- Serial_No:03201317:51 Page 62 of 78 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 Date Analyzed Analytical Method Analyst Date Prepared 03/20/13 Nitrogen, Nitrate Chloride Cyanide, Total Chemical Oxygen Demand Alkalinity, Total Solids, Total Dissolved Sulfate ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg CaCO3/L mg/l mg/l 1 1 1 1 1 1 1 0.100 1.0 0.005 20 2.00 10 10 03/13/13 21:51 03/14/13 11:06 03/14/13 15:22 03/14/13 21:20 03/15/13 09:28 03/18/13 12:15 03/18/13 15:45 30,4500NO3-F 1,9251 1,9010C/9012A 30,5220D 30,2320B 30,2540C 1,9038 DB LA JO TL SD DW MP - - 03/14/13 10:05 03/14/13 17:30 - - 03/18/13 15:45 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595146-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595209-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595310-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595382-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595622-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595781-1 General Chemistry - Westborough Lab for sample(s): 01-08 Batch: WG595883-1 MDL -- -- -- -- NA -- -- Serial_No:03201317:51 Page 63 of 78 Nitrogen, Nitrate Chloride Cyanide, Total Chemical Oxygen Demand Alkalinity, Total Solids, Total Dissolved Sulfate 100 90 104 99 103 95 90 - - 120 - - - - 90-110 90-110 80-120 93-106 90-110 80-120 84-119 - - 14 - - - - 20 10 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595146-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595209-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595310-2 WG595310-3 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595382-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595622-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595781-2 General Chemistry - Westborough Lab Associated sample(s): 01-08 Batch: WG595883-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Qual Qual Serial_No:03201317:51 Page 64 of 78 Nitrogen, Nitrate Chloride Cyanide, Total Chemical Oxygen Demand Alkalinity, Total Sulfate 0.157 400 0.013 ND 17.4 44 4.19 410 0.196 240 124 140 101 50 92 101 107 96 - - 0.195 - - - - - 91 - - - 83-113 58-140 80-120 84-120 86-116 55-147 - - 1 - - - 17 7 20 12 10 14 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595146-4 QC Sample: L1304142-01 Client ID: MW-5S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595209-4 QC Sample: L1304142-02 Client ID: MW-5D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595310-4 WG595310-5 QC Sample: L1304142-02 Client ID: MW- 5D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595382-3 QC Sample: L1304142-06 Client ID: MW-1D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595622-3 QC Sample: L1304142-08 Client ID: MW-8D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595883-4 QC Sample: L1304142-02 Client ID: MW-5D 4 20 0.2 238 100 100 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LANDFILL 1910-88908-CG.SAMP L1304142 03/20/13 Qual Q Qual Qual Serial_No:03201317:51 Page 65 of 78 Nitrogen, Nitrate Chloride Chemical Oxygen Demand Alkalinity, Total Solids, Total Dissolved Sulfate 0.157 400 ND 17.4 1000 ND 0.159 390 ND 17.4 1000 ND mg/l mg/l mg/l mg CaCO3/L mg/l mg/l 0 3 NC 0 0 NC 17 7 12 10 20 14 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595146-3 QC Sample: L1304142-01 Client ID: MW-5S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595209-3 QC Sample: L1304142-02 Client ID: MW-5D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595382-4 QC Sample: L1304142-06 Client ID: MW-1D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595622-4 QC Sample: L1304142-08 Client ID: MW-8D General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595781-3 QC Sample: L1304142-07 Client ID: MW-8S General Chemistry - Westborough Lab Associated sample(s): 01-08 QC Batch ID: WG595883-3 QC Sample: L1304142-01 Client ID: MW-5S NANTUCKET LANDFILL 1910-88908-CG.SA Project Name: Project Number: L1304142Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 03/20/13 Qual Serial_No:03201317:51 Page 66 of 78 *Values in parentheses indicate holding time in days L1304142-01A L1304142-01B L1304142-01C L1304142-01D L1304142-01E L1304142-01F L1304142-01G L1304142-01H L1304142-02A L1304142-02B L1304142-02C L1304142-02D L1304142-02E L1304142-02F L1304142-02G L1304142-02H L1304142-03A Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved B B B B B B B B B B B B B B B B B N/A N/A N/A <2 >12 N/A <2 7 N/A N/A N/A <2 >12 N/A <2 7 N/A 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A B Absent Absent Cooler Custody SealCooler Information NANTUCKET LANDFILL 1910-88908-CG.SAMP 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) Project Name: Project Number: L1304142Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/20/13 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:03201317:51 Page 67 of 78 *Values in parentheses indicate holding time in days L1304142-03B L1304142-03C L1304142-03D L1304142-03E L1304142-03F L1304142-03G L1304142-03H L1304142-04A L1304142-04B L1304142-04C L1304142-04D L1304142-04E L1304142-04F L1304142-04G L1304142-04H L1304142-05A L1304142-05B L1304142-05C L1304142-05D L1304142-05E L1304142-05F L1304142-05G L1304142-05H Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved B B B B B B B B B B B B B B B A A A A A A A A N/A N/A <2 >12 N/A <2 7 N/A N/A N/A <2 >12 N/A <2 7 N/A N/A N/A <2 >12 N/A <2 7 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LANDFILL 1910-88908-CG.SAMP 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) Project Name: Project Number: L1304142Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/20/13 Serial_No:03201317:51 Page 68 of 78 *Values in parentheses indicate holding time in days L1304142-06A L1304142-06B L1304142-06C L1304142-06D L1304142-06E L1304142-06F L1304142-06G L1304142-06H L1304142-07A L1304142-07B L1304142-07C L1304142-07D L1304142-07E L1304142-07F L1304142-07G L1304142-07H L1304142-08A L1304142-08B L1304142-08C L1304142-08D L1304142-08E L1304142-08F L1304142-08G Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml unpreserved Plastic 500ml HNO3 preserved A A A A A A A A A A A A A A A A A A A A A A A N/A N/A N/A <2 >12 N/A <2 7 N/A N/A N/A <2 >12 N/A <2 7 N/A N/A N/A <2 >12 N/A <2 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LANDFILL 1910-88908-CG.SAMP 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) COD-5220(28) TCN-9010(14) ALK-T-2320(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) Project Name: Project Number: L1304142Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/20/13 Serial_No:03201317:51 Page 69 of 78 *Values in parentheses indicate holding time in days L1304142-08H L1304142-09A Plastic 500ml unpreserved Vial HCl preserved A A 7 N/A 4 4 Y Y Absent Absent NANTUCKET LANDFILL 1910-88908-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) Project Name: Project Number: L1304142Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/20/13 Serial_No:03201317:51 Page 70 of 78 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1304142NANTUCKET LANDFILL 1910-88908-CG.SAMP 03/20/13 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G H I - - - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reported 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:03201317:51 Page 71 of 78 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1304142NANTUCKET LANDFILL 1910-88908-CG.SAMP 03/20/13 Data Qualifiers M NJ P Q R RE - - - - - - due to obvious interference. Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:03201317:51 Page 72 of 78 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1304142NANTUCKET LANDFILL 1910-88908-CG.SAMP REFERENCES 03/20/13 Serial_No:03201317:51 Page 73 of 78 Certificate/Approval Program Summary Last revised December 19, 2012 - Westboro Facility The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative. Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4- Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O- Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl- D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 6010C, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8330, 8151A, 8260B, 8260C, 8270C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9030B, 9040B, 9045C, 6010B, 6010C, 6020, 6020A, 7471A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8270D, 8330, 8151A, 8081A, 8081B, 8082, 8082A, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2- Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Serial_No:03201317:51 Page 74 of 78 Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW- 846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, LACHAT 10-204- 00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010C, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012B, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C, Serial_No:03201317:51 Page 75 of 78 3546, 3580A, 5030B, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F- C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D- SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL- E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 355B0, 3580A, 3630C, 6020A, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C, Serial_No:03201317:51 Page 76 of 78 8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Serial_No:03201317:51 Page 77 of 78 Serial_No:03201317:51 Page 78 of 78 L1304045 CDM Smith, Inc. 1910-97168-CG.SAMP NANTUCKET LF Client: Project Name: Project Number: 03/18/13 Eight Walkup Drive, Westborough, MA 01581-1019 Lab Number: Report Date: 508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com 1 Cambridge Place 50 Hampshire Street Laura BugayATTN: ANALYTICAL REPORT Certifications & Approvals: MA (M-MA086), NY (11148), CT (PH-0574), NH (2003), NJ NELAP (MA935), RI (LAO00065), ME (MA00086), PA (68-03671), USDA (Permit #P-330-11-00240), NC (666), TX (T104704476), DOD (L2217), US Army Corps of Engineers. Cambridge, MA 02139 (617) 452-6589Phone: The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original. Serial_No:03181313:41 Page 1 of 87 L1304045-01 L1304045-02 L1304045-03 L1304045-04 L1304045-05 L1304045-06 L1304045-07 L1304045-08 L1304045-09 L1304045-10 Alpha Sample ID MW-3S MW-3D MW-7S MW-7D DUP-1 FB-1 SW-1 SW-2 SW-3 TRIP BLANK Client ID NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA NANTUCKET, MA Sample Location NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304045 03/18/13 03/11/13 13:00 03/11/13 13:30 03/11/13 15:45 03/11/13 16:00 03/11/13 00:00 03/11/13 15:15 03/11/13 15:00 03/11/13 14:30 03/11/13 14:00 03/11/13 00:00 Collection Date/Time Serial_No:03181313:41 Page 2 of 87 NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304045 03/18/13 Case Narrative The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report. Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed along with any associated usability implications. Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical Standards requested on the Chain of Custody. HOLD POLICY For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30 days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and made arrangements for Alpha to continue to hold the samples. Please contact Client Services at 800-624-9220 with any questions. Serial_No:03181313:41 Page 3 of 87 Case Narrative (continued) NANTUCKET LF 1910-97168-CG.SAMP Project Name: Project Number: Lab Number: Report Date: L1304045 03/18/13 Sample Receipt L1304045-02 through -05, -07, -08, and -09 were received below the appropriate pH for the Cyanide analysis. The laboratory added additional NaOH to a pH >12. Metals L1304045-02, -03, and -08 have elevated detection limits for Arsenic due to the dilutions required by matrix interferences encountered during analysis. L1304045-07 has elevated detection limits for Cadmium, Copper, Lead, and Silver due to the dilution required by matrix interferences encountered during analysis. The WG595347-3 Laboratory Duplicate RPD, performed on L1304045-09, is above the acceptance criteria for Silver (45%); however, the sample and duplicate results are less than five times the reporting limit. Therefore, the RPD is valid. I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report. Authorized Signature: Title: Technical Director/Representative Date: 03/18/13 Serial_No:03181313:41 Page 4 of 87 ORGANICS Serial_No:03181313:41 Page 5 of 87 VOLATILES Serial_No:03181313:41 Page 6 of 87 FF Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 MW-3SClient ID: 03/11/13 13:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-01Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 14:36 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 7 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 MW-3SClient ID: 03/11/13 13:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 8 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 110 99 111 98 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 MW-3SClient ID: 03/11/13 13:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-01Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 9 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 MW-3DClient ID: 03/11/13 13:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-02Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 15:11 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 10 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 MW-3DClient ID: 03/11/13 13:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 11 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 111 99 108 100 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 MW-3DClient ID: 03/11/13 13:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-02Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 12 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 MW-7SClient ID: 03/11/13 15:45Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-03Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 15:47 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 13 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 MW-7SClient ID: 03/11/13 15:45Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 14 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 98 107 99 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 MW-7SClient ID: 03/11/13 15:45Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-03Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 15 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 MW-7DClient ID: 03/11/13 16:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-04Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 16:23 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 16 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 MW-7DClient ID: 03/11/13 16:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 17 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 114 99 108 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 MW-7DClient ID: 03/11/13 16:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-04Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 18 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 DUP-1Client ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-05Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 16:58 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 19 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 DUP-1Client ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 20 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 99 108 98 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 DUP-1Client ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-05Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 21 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 FB-1Client ID: 03/11/13 15:15Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-06Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 17:34 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 22 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 FB-1Client ID: 03/11/13 15:15Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 23 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 99 107 97 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 FB-1Client ID: 03/11/13 15:15Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-06Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 24 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-07Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 18:10 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 25 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 26 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 116 99 109 100 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-07Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 27 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 SW-2Client ID: 03/11/13 14:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-08Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 18:45 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 28 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 SW-2Client ID: 03/11/13 14:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 29 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 99 109 100 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 SW-2Client ID: 03/11/13 14:30Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-08Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 30 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 SW-3Client ID: 03/11/13 14:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-09Lab ID: Field Prep:See Narrative Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 19:20 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 31 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 SW-3Client ID: 03/11/13 14:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-09Lab ID: Field Prep:See Narrative MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 32 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 110 99 108 99 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 SW-3Client ID: 03/11/13 14:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-09Lab ID: Field Prep:See Narrative MDL -- -- -- -- Serial_No:03181313:41 Page 33 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 03/18/13 TRIP BLANKClient ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-10Lab ID: Field Prep:Not Specified Matrix:Water Analytical Method: Analytical Date: Analyst: 1,8260C 03/13/13 19:56 PD MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 34 of 87 Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene Parameter Result Dilution Factor ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 03/18/13 TRIP BLANKClient ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-10Lab ID: Field Prep:Not Specified MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 35 of 87 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result Dilution Factor ND ND ND ND ug/l ug/l ug/l ug/l 1 1 1 1 Qualifier Units RL Volatile Organics by GC/MS - Westborough Lab SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 2.5 2.5 2.5 250 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 113 100 111 99 70-130 70-130 70-130 70-130 Acceptance CriteriaSurrogate % Recovery Qualifier 03/18/13 TRIP BLANKClient ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: NANTUCKET, MASample Location: L1304045-10Lab ID: Field Prep:Not Specified MDL -- -- -- -- Serial_No:03181313:41 Page 36 of 87 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/13/13 14:00 1,8260CAnalytical Method: Analytical Date: 03/18/13 Analyst:PD Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 3.0 0.75 0.75 0.50 1.8 0.50 0.75 0.50 0.50 2.5 0.50 0.50 0.50 0.50 0.50 2.5 2.0 0.50 0.50 0.75 0.50 2.5 1.0 1.0 1.0 0.50 0.75 0.50 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-10 Batch: WG595214-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 37 of 87 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/13/13 14:00 1,8260CAnalytical Method: Analytical Date: 03/18/13 Analyst:PD Methyl tert butyl ether p/m-Xylene o-Xylene Xylenes, Total cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND RL 1.0 1.0 1.0 1.0 0.50 5.0 5.0 5.0 1.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 5.0 2.5 5.0 2.5 2.0 2.5 0.50 2.5 0.50 0.50 2.5 2.5 2.5 2.5 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-10 Batch: WG595214-3 MDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 38 of 87 Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/13/13 14:00 1,8260CAnalytical Method: Analytical Date: 03/18/13 Analyst:PD Hexachlorobutadiene Isopropylbenzene p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane Parameter Result ND ND ND ND ND ND ND ND ND ND ND ND RL 0.50 0.50 0.50 2.5 0.50 2.5 2.5 2.5 2.5 2.5 2.5 250 ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l ug/l UnitsQualifier Volatile Organics by GC/MS - Westborough Lab for sample(s): 01-10 Batch: WG595214-3 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 112 99 113 100 70-130 70-130 70-130 70-130 Surrogate %Recovery Qualifier Acceptance Criteria MDL -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 39 of 87 Methylene chloride 1,1-Dichloroethane Chloroform Carbon tetrachloride 1,2-Dichloropropane Dibromochloromethane 1,1,2-Trichloroethane Tetrachloroethene Chlorobenzene Trichlorofluoromethane 1,2-Dichloroethane 1,1,1-Trichloroethane Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene 1,1-Dichloropropene Bromoform 1,1,2,2-Tetrachloroethane Benzene Toluene Ethylbenzene 88 97 100 93 99 95 96 100 96 111 104 101 104 88 91 100 104 97 98 95 103 96 107 111 101 103 103 103 107 104 117 112 111 114 96 98 107 115 106 104 101 110 70-130 70-130 70-130 63-132 70-130 63-130 70-130 70-130 75-130 62-150 70-130 67-130 67-130 70-130 70-130 70-130 54-136 67-130 70-130 70-130 70-130 9 10 10 8 4 8 7 7 8 5 7 9 9 9 7 7 10 9 6 6 7 20 20 20 20 20 20 20 20 25 20 20 20 20 20 20 20 20 20 25 25 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-10 Batch: WG595214-1 WG595214-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 40 of 87 Chloromethane Bromomethane Vinyl chloride Chloroethane 1,1-Dichloroethene trans-1,2-Dichloroethene Trichloroethene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene Dibromomethane 1,4-Dichlorobutane 1,2,3-Trichloropropane Styrene Dichlorodifluoromethane Acetone Carbon disulfide 70 91 105 100 95 94 98 95 96 95 88 98 99 91 101 95 96 104 81 124 97 72 95 112 106 101 101 106 104 104 103 98 105 106 100 109 102 103 113 86 124 105 64-130 39-139 55-140 55-138 61-145 70-130 70-130 70-130 70-130 70-130 63-130 70-130 70-130 70-130 70-130 70-130 64-130 70-130 36-147 58-148 51-130 3 4 6 6 6 7 8 9 8 8 11 7 7 9 8 7 7 8 6 0 8 20 20 20 20 25 20 25 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-10 Batch: WG595214-1 WG595214-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 41 of 87 2-Butanone Vinyl acetate 4-Methyl-2-pentanone 2-Hexanone Ethyl methacrylate Acrylonitrile Bromochloromethane Tetrahydrofuran 2,2-Dichloropropane 1,2-Dibromoethane 1,3-Dichloropropane 1,1,1,2-Tetrachloroethane Bromobenzene n-Butylbenzene sec-Butylbenzene tert-Butylbenzene o-Chlorotoluene p-Chlorotoluene 1,2-Dibromo-3-chloropropane Hexachlorobutadiene Isopropylbenzene 103 100 94 105 93 95 95 96 84 98 98 95 97 100 101 96 100 99 97 96 100 106 109 104 109 102 104 103 104 90 104 104 103 104 110 110 104 108 107 111 105 109 63-138 70-130 59-130 57-130 70-130 70-130 70-130 58-130 63-133 70-130 70-130 64-130 70-130 53-136 70-130 70-130 70-130 70-130 41-144 63-130 70-130 3 9 10 4 9 9 8 8 7 6 6 8 7 10 9 8 8 8 13 9 9 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-10 Batch: WG595214-1 WG595214-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 42 of 87 p-Isopropyltoluene Naphthalene n-Propylbenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene trans-1,4-Dichloro-2-butene Ethyl ether 1,4-Dioxane 99 81 102 88 86 100 100 94 101 97 108 93 110 98 96 108 110 99 107 108 70-130 70-130 69-130 70-130 70-130 64-130 70-130 70-130 59-134 56-162 9 14 8 11 11 8 10 5 6 11 20 20 20 20 20 20 20 20 20 20 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 01-10 Batch: WG595214-1 WG595214-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene Dibromofluoromethane 105 99 97 101 70-130 70-130 70-130 70-130 106 98 98 101 Surrogate Qual%Recovery Qual%Recovery LCS LCSD 03/18/13 Acceptance Criteria Qual Qual Qual Serial_No:03181313:41 Page 43 of 87 METALS Serial_No:03181313:41 Page 44 of 87 FF Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS MW-3SClient ID: 03/11/13 13:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-01Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0292 ND 40. ND 0.0328 0.28 ND 0.0160 ND ND ND 62. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/15/13 09:59 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 03/14/13 18:22 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 45 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS MW-3DClient ID: 03/11/13 13:30Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-02Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0208 ND 39. ND ND 0.22 ND 0.884 ND ND ND 57. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 2 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0100 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/15/13 10:03 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/15/13 10:04 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 03/14/13 18:25 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MS KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 46 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS MW-7SClient ID: 03/11/13 15:45Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-03Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0931 ND 290 ND ND 68. ND 1.93 ND ND ND 110 0.405 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 10 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0500 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/15/13 10:14 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/15/13 10:06 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 03/14/13 18:29 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C MS KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 47 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS MW-7DClient ID: 03/11/13 16:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-04Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0112 ND 19. ND ND 1.5 ND 0.0810 ND ND ND 24. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/15/13 10:08 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 03/14/13 18:33 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 48 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS DUP-1Client ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-05Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND 0.0203 ND 39. ND ND 0.23 ND 0.885 ND ND ND 57. ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/15/13 10:10 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 03/14/13 18:37 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 49 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS FB-1Client ID: 03/11/13 15:15Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-06Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.00020 0.0100 0.0070 2.0 0.0500 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/15/13 10:16 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 03/14/13 18:48 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL KL KL JH KL KL KL KL 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 50 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Total Hardness by SM 2340B - Westborough Lab Dissolved Metals - Westborough Lab Hardness Arsenic, Dissolved Barium, Dissolved Calcium, Dissolved Chromium, Dissolved Iron, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Sodium, Dissolved Zinc, Dissolved 1900 ND 0.0142 140 ND ND 0.0970 ND ND 3500 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 10 1 0.66 0.0050 0.0100 0.10 0.010 0.050 0.0100 0.00020 0.0100 20. 0.0500 03/13/13 19:21 03/14/13 18:52 03/14/13 18:52 03/14/13 18:52 03/14/13 18:52 03/14/13 18:52 03/14/13 18:52 03/15/13 10:18 03/14/13 18:52 03/15/13 10:18 03/14/13 18:52 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,7470A 1,6010C 1,6010C 1,6010C KL KL KL KL KL KL KL JH KL MS KL 03/13/13 10:33 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 EPA 3005A NA NA NA NA NA NA EPA 7470A NA NA NA Prep MethodMDL NA -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 51 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-07Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Dissolved Metals - Westborough Lab Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved ND ND ND ND mg/l mg/l mg/l mg/l 10 10 10 10 0.00200 0.01000 0.00500 0.00400 03/15/13 11:24 03/15/13 11:24 03/15/13 11:24 03/15/13 11:24 1,6020A 1,6020A 1,6020A 1,6020A AK AK AK AK 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 NA NA NA NA Prep Method D MDL -- -- -- -- Serial_No:03181313:41 Page 52 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS SW-2Client ID: 03/11/13 14:30Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-08Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Total Hardness by SM 2340B - Westborough Lab Dissolved Metals - Westborough Lab Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 430 ND 0.0531 ND 140 ND 0.00327 3.2 ND 0.338 ND ND 0.00066 120 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 2 1 1 1 1 1 1 1 1 1 1 1 1 1 0.66 0.0100 0.0100 0.00020 0.10 0.010 0.00100 0.050 0.00050 0.0100 0.00020 0.0100 0.00040 2.0 0.0500 03/13/13 19:33 03/15/13 10:22 03/14/13 18:56 03/15/13 11:31 03/14/13 18:56 03/14/13 18:56 03/15/13 11:31 03/14/13 18:56 03/15/13 11:31 03/14/13 18:56 03/15/13 10:20 03/14/13 18:56 03/15/13 11:31 03/14/13 18:56 03/14/13 18:56 1,6010C 1,6010C 1,6010C 1,6020A 1,6010C 1,6010C 1,6020A 1,6010C 1,6020A 1,6010C 1,7470A 1,6010C 1,6020A 1,6010C 1,6010C KL MS KL AK KL KL AK KL AK KL JH KL AK KL KL 03/13/13 10:33 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 EPA 3005A NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 53 of 87 Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 SAMPLE RESULTS SW-3Client ID: 03/11/13 14:00Date Collected: 03/12/13Date Received: Matrix:Water NANTUCKET, MASample Location: L1304045-09Lab ID: Field Prep:See Narrative Parameter Result Dilution FactorQualifierUnitsRL Date Analyzed Analytical Method Analyst Date Prepared Total Hardness by SM 2340B - Westborough Lab Dissolved Metals - Westborough Lab Hardness Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Mercury, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 100 ND 0.0397 0.00049 25. ND 0.01146 0.13 0.00131 0.0107 ND ND 0.00084 58. 0.191 mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.66 0.0050 0.0100 0.00020 0.10 0.010 0.00100 0.050 0.00050 0.0100 0.00020 0.0100 0.00040 2.0 0.0500 03/13/13 19:36 03/14/13 18:10 03/14/13 18:10 03/15/13 11:11 03/14/13 18:10 03/14/13 18:10 03/15/13 11:11 03/14/13 18:10 03/15/13 11:11 03/14/13 18:10 03/15/13 10:21 03/14/13 18:10 03/15/13 11:11 03/14/13 18:10 03/14/13 18:10 1,6010C 1,6010C 1,6010C 1,6020A 1,6010C 1,6010C 1,6020A 1,6010C 1,6020A 1,6010C 1,7470A 1,6010C 1,6020A 1,6010C 1,6010C KL KL KL AK KL KL AK KL AK KL JH KL AK KL KL 03/13/13 10:33 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 19:41 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 EPA 3005A NA NA NA NA NA NA NA NA NA EPA 7470A NA NA NA NA Prep MethodMDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 54 of 87 FF Parameter Parameter Parameter Result Result Result Dilution Factor Dilution Factor Dilution Factor Qualifier Qualifier Qualifier Units Units Units RL RL RL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Date Analyzed Date Analyzed Date Analyzed Analytical Method Analytical Method Analytical Method Analyst Analyst Analyst Date Prepared Date Prepared Date Prepared 03/18/13 Hardness Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 0.66 0.00020 0.00100 0.00050 0.00040 0.0050 0.0100 0.0050 0.10 0.010 0.0100 0.050 0.0100 0.0100 0.0100 0.0070 2.0 0.0500 03/13/13 19:06 03/15/13 10:54 03/15/13 10:54 03/15/13 10:54 03/15/13 10:54 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 03/14/13 18:03 1,6010C 1,6020A 1,6020A 1,6020A 1,6020A 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C 1,6010C KL AK AK AK AK KL KL KL KL KL KL KL KL KL KL KL KL KL 03/13/13 10:33 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 03/14/13 14:50 Total Hardness by SM 2340B - Westborough Lab for sample(s): 07-09 Batch: WG594990-1 Dissolved Metals - Westborough Lab for sample(s): 07-09 Batch: WG595347-1 Dissolved Metals - Westborough Lab for sample(s): 01-09 Batch: WG595348-1 EPA 3005A NA Digestion Method: Digestion Method: Prep Information Prep Information MDL MDL MDL NA -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Serial_No:03181313:41 Page 55 of 87 Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Date Analyzed Analytical Method Analyst Date Prepared 03/18/13 Mercury, Dissolved ND mg/l 10.00020 03/15/13 09:55 1,7470A JH03/14/13 19:41 Dissolved Metals - Westborough Lab for sample(s): 01-09 Batch: WG595373-1 NA EPA 7470A Digestion Method: Digestion Method: Prep Information Prep Information MDL -- Serial_No:03181313:41 Page 56 of 87 Hardness Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved 100 105 99 100 87 - - - - - 80-120 80-120 80-120 80-120 80-120 - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07-09 Batch: WG594990-2 Dissolved Metals - Westborough Lab Associated sample(s): 07-09 Batch: WG595347-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 57 of 87 Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved 102 94 101 100 95 91 96 95 94 99 95 110 94 82 - - - - - - - - - - - - - - 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 80-120 70-130 - - - - - - - - - - - - - - Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-09 Batch: WG595348-2 Dissolved Metals - Westborough Lab Associated sample(s): 01-09 Batch: WG595373-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Serial_No:03181313:41 Page 58 of 87 Hardness Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Arsenic, Dissolved Barium, Dissolved Cadmium, Dissolved Calcium, Dissolved Chromium, Dissolved Copper, Dissolved Iron, Dissolved Lead, Dissolved Manganese, Dissolved Selenium, Dissolved Silver, Dissolved Sodium, Dissolved Zinc, Dissolved 30 0.00049 0.01146 0.00131 0.00084 ND 0.0397 ND 25 ND ND 0.13 ND 0.0107 ND ND 58 0.191 93 0.05481 0.2534 0.5114 0.04283 0.128 1.93 0.0520 34 0.19 0.244 1.1 0.484 0.465 0.127 0.0478 67 0.660 95 106 97 100 84 107 94 102 90 95 98 97 95 91 106 96 90 94 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 75-125 80-120 80-120 80-120 80-120 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 - - - - - - - - - - - - - - - - - - 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07-09 QC Batch ID: WG594990-4 QC Sample: L1304062-02 Client ID: MS Sample Dissolved Metals - Westborough Lab Associated sample(s): 07-09 QC Batch ID: WG595347-4 QC Sample: L1304045-09 Client ID: SW-3 Dissolved Metals - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595348-4 QC Sample: L1304045-09 Client ID: SW-3 66.2 0.051 0.25 0.51 0.05 0.12 2 0.051 10 0.2 0.25 1 0.51 0.5 0.12 0.05 10 0.5 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 59 of 87 Mercury, Dissolved ND 0.00101 101 --70-130 -20 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits Dissolved Metals - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595373-4 QC Sample: L1304045-01 Client ID: MW-3S 0.001 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Serial_No:03181313:41 Page 60 of 87 Hardness Cadmium, Dissolved Copper, Dissolved Lead, Dissolved Silver, Dissolved Arsenic, Dissolved Barium, Dissolved Calcium, Dissolved Chromium, Dissolved Iron, Dissolved Manganese, Dissolved Selenium, Dissolved Sodium, Dissolved Zinc, Dissolved Mercury, Dissolved 30 0.00049 0.01146 0.00131 0.00084 ND 0.0397 25 ND 0.13 0.0107 ND 58 0.191 ND 32. 0.00051 0.01103 0.00128 0.00053 ND 0.0390 25. ND 0.12 0.0100 ND 58. 0.188 ND mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l 6 5 4 2 45 NC 2 0 NC 8 7 NC 0 2 NC 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Units RPDParameterNative Sample Duplicate Sample RPD Limits Total Hardness by SM 2340B - Westborough Lab Associated sample(s): 07-09 QC Batch ID: WG594990-3 QC Sample: L1304062-02 Client ID: DUP Sample Dissolved Metals - Westborough Lab Associated sample(s): 07-09 QC Batch ID: WG595347-3 QC Sample: L1304045-09 Client ID: SW-3 Dissolved Metals - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595348-3 QC Sample: L1304045-09 Client ID: SW-3 Dissolved Metals - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595373-3 QC Sample: L1304045-01 Client ID: MW-3S NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1304045Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 03/18/13 Qual Q Serial_No:03181313:41 Page 61 of 87 INORGANICS & MISCELLANEOUS Serial_No:03181313:41 Page 62 of 87 FF MW-3SClient ID: 03/11/13 13:00Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-01Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 153. 550 ND 63. 7.12 99. 160 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 5 1 2.00 10 0.005 1.0 0.100 50 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:01 03/14/13 11:02 03/12/13 22:00 03/14/13 14:30 03/13/13 20:43 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 63 of 87 FF MW-3DClient ID: 03/11/13 13:30Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-02Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 162. 400 ND 69. ND 67. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:01 03/14/13 11:03 03/12/13 22:47 03/14/13 14:30 03/13/13 20:43 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 64 of 87 FF MW-7SClient ID: 03/11/13 15:45Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-03Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 747. 1700 0.040 90. 1.37 550 150 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 2 1 1 5 1 25 1 4.00 10 0.005 5.0 0.100 250 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:02 03/14/13 11:46 03/12/13 22:03 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 65 of 87 FF MW-7DClient ID: 03/11/13 16:00Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-04Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 73.5 210 ND 33. ND 52. ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:06 03/14/13 11:07 03/12/13 22:04 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 66 of 87 FF DUP-1Client ID: 03/11/13 00:00Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-05Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 164. 400 ND 70. ND 79. 21. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:07 03/14/13 11:08 03/12/13 22:07 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 67 of 87 FF FB-1Client ID: 03/11/13 15:15Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-06Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand ND ND ND ND ND ND ND mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 1 1 2.00 10 0.005 1.0 0.100 10 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:08 03/14/13 11:09 03/12/13 22:07 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 68 of 87 FF SW-1Client ID: 03/11/13 15:00Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-07Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 58.1 13000 ND 7000 0.119 950 540 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 100 1 25 1 2.00 10 0.005 100 0.100 250 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:08 03/14/13 11:48 03/12/13 22:08 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 69 of 87 FF SW-2Client ID: 03/11/13 14:30Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-08Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 240. 990 ND 190 0.444 220 130 mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 10 1 10 1 2.00 10 0.005 10 0.100 100 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:09 03/14/13 11:50 03/12/13 22:09 03/14/13 14:30 03/13/13 20:44 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 70 of 87 FF SW-3Client ID: 03/11/13 14:00Date Collected: 03/12/13Date Received: Parameter Result Dilution Factor Matrix:Water NANTUCKET, MASample Location: L1304045-09Lab ID: Qualifier Units RL SAMPLE RESULTS Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Field Prep: Date Analyzed Analytical Method Analyst See Narrative General Chemistry - Westborough Lab Alkalinity, Total Solids, Total Dissolved Cyanide, Total Chloride Nitrogen, Nitrate Sulfate Chemical Oxygen Demand 92.3 370 ND 80. 1.01 56. 58. mg CaCO3/L mg/l mg/l mg/l mg/l mg/l mg/l 1 1 1 1 1 2 1 2.00 10 0.005 1.0 0.100 20 20 03/15/13 09:28 03/13/13 14:20 03/18/13 12:10 03/14/13 11:51 03/12/13 22:09 03/14/13 14:30 03/13/13 20:45 30,2320B 30,2540C 1,9010C/9012A 1,9251 30,4500NO3-F 1,9038 30,5220D SD DW DE LA DB MP TL Date Prepared - - 03/14/13 21:45 - - 03/14/13 14:30 03/12/13 17:25 03/18/13 MDL NA -- -- -- -- -- -- Serial_No:03181313:41 Page 71 of 87 FF Parameter Result Dilution FactorQualifierUnitsRL Method Blank Analysis Batch Quality Control Project Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 Date Analyzed Analytical Method Analyst Date Prepared 03/18/13 Nitrogen, Nitrate Solids, Total Dissolved Cyanide, Total Chemical Oxygen Demand Chloride Sulfate Alkalinity, Total ND ND ND ND ND ND ND mg/l mg/l mg/l mg/l mg/l mg/l mg CaCO3/L 1 1 1 1 1 1 1 0.100 10 0.005 20 1.0 10 2.00 03/12/13 21:37 03/13/13 14:20 03/18/13 11:57 03/13/13 20:38 03/14/13 11:00 03/14/13 14:30 03/15/13 09:28 30,4500NO3-F 30,2540C 1,9010C/9012A 30,5220D 1,9251 1,9038 30,2320B DB DW DE TL LA MP SD - - 03/14/13 21:45 03/12/13 17:25 - 03/14/13 14:30 - General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG594872-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG594943-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG594992-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG595122-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG595208-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG595272-1 General Chemistry - Westborough Lab for sample(s): 01-09 Batch: WG595618-1 MDL -- -- -- -- -- -- NA Serial_No:03181313:41 Page 72 of 87 Nitrogen, Nitrate Solids, Total Dissolved Cyanide, Total Chemical Oxygen Demand Chloride Sulfate Alkalinity, Total 99 96 101 102 90 100 105 - - 101 - - - - 90-110 80-120 80-120 93-106 90-110 84-119 90-110 - - 0 - - - - 20 10 Parameter LCS %Recovery LCSD %Recovery %Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG594872-2 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG594943-2 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG594992-2 WG594992-3 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG595122-2 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG595208-2 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG595272-2 General Chemistry - Westborough Lab Associated sample(s): 01-09 Batch: WG595618-2 Lab Control Sample Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 73 of 87 Nitrogen, Nitrate Cyanide, Total Chemical Oxygen Demand Chloride Sulfate Alkalinity, Total 7.12 0.040 ND 62 17 79.1 10.9 0.243 250 81 39 184 94 101 105 95 110 105 - 0.245 - - - - - 102 - - - - 83-113 80-120 84-120 58-140 55-147 86-116 - 1 - - - - 17 20 12 7 14 10 Parameter Native Sample MS Found MS %Recovery MSD Found MSD %Recovery Recovery Limits RPD RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG594872-4 QC Sample: L1304045-01 Client ID: MW-3S General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG594992-4 WG594992-5 QC Sample: L1304045-03 Client ID: MW- 7S General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595122-3 QC Sample: L1304045-04 Client ID: MW-7D General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595208-4 QC Sample: L1304084-06 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595272-4 QC Sample: L1303960-06 Client ID: MS Sample General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595618-3 QC Sample: L1304113-01 Client ID: MS Sample 4 0.2 238 20 20 100 MS Added Matrix Spike Analysis Batch Quality ControlProject Name: Project Number: Lab Number: Report Date: NANTUCKET LF 1910-97168-CG.SAMP L1304045 03/18/13 Qual Qual Qual Serial_No:03181313:41 Page 74 of 87 Nitrogen, Nitrate Solids, Total Dissolved Chemical Oxygen Demand Chloride Sulfate Alkalinity, Total 7.12 550 ND 62 ND 79.1 7.10 530 ND 63. ND 78.6 mg/l mg/l mg/l mg/l mg/l mg CaCO3/L 0 4 NC 2 NC 1 17 20 12 7 14 10 Units RPDParameterNative Sample Duplicate Sample RPD Limits General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG594872-3 QC Sample: L1304045-01 Client ID: MW-3S General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG594943-3 QC Sample: L1304045-01 Client ID: MW-3S General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595122-4 QC Sample: L1304045-04 Client ID: MW-7D General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595208-3 QC Sample: L1304084-06 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595272-3 QC Sample: L1303960-01 Client ID: DUP Sample General Chemistry - Westborough Lab Associated sample(s): 01-09 QC Batch ID: WG595618-4 QC Sample: L1304113-01 Client ID: DUP Sample NANTUCKET LF 1910-97168-CG.SA Project Name: Project Number: L1304045Lab Number: Report Date: Lab Duplicate Analysis Batch Quality Control 03/18/13 Qual Serial_No:03181313:41 Page 75 of 87 *Values in parentheses indicate holding time in days L1304045-01A L1304045-01B L1304045-01C L1304045-01D L1304045-01E L1304045-01F L1304045-01G L1304045-01H L1304045-02A L1304045-02B L1304045-02C L1304045-02D L1304045-02E L1304045-02F L1304045-02G L1304045-02H L1304045-03A L1304045-03B Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved A A A A A A A A A A A A A A A A A A N/A N/A N/A N/A <2 >12 <2 6 N/A N/A N/A N/A <2 >12 <2 6 N/A N/A 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent A Absent Cooler Custody SealCooler Information NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) Project Name: Project Number: L1304045Lab Number: Report Date: Sample Receipt and Container Information Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/18/13 Were project specific reporting limits specified?YES Reagent H2O Preserved Vials Frozen on:NA Serial_No:03181313:41 Page 76 of 87 *Values in parentheses indicate holding time in days L1304045-03C L1304045-03D L1304045-03E L1304045-03F L1304045-03G L1304045-03H L1304045-04A L1304045-04B L1304045-04C L1304045-04D L1304045-04E L1304045-04F L1304045-04G L1304045-04H L1304045-05A L1304045-05B L1304045-05C L1304045-05D L1304045-05E L1304045-05F L1304045-05G L1304045-05H L1304045-06A Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved A A A A A A A A A A A A A A A A A A A A A A A N/A N/A <2 >12 <2 6 N/A N/A N/A N/A <2 >12 <2 6 N/A N/A N/A N/A <2 >12 <2 6 N/A 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) Project Name: Project Number: L1304045Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/18/13 Serial_No:03181313:41 Page 77 of 87 *Values in parentheses indicate holding time in days L1304045-06B L1304045-06C L1304045-06D L1304045-06E L1304045-06F L1304045-06G L1304045-06H L1304045-07A L1304045-07B L1304045-07C L1304045-07D L1304045-07E L1304045-07F L1304045-07G L1304045-07H L1304045-07I L1304045-08A L1304045-08B L1304045-08C L1304045-08D L1304045-08E L1304045-08F L1304045-08G L1304045-08H Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml HNO3 preserved A A A A A A A A A A A A A A A A A A A A A A A A N/A N/A N/A <2 >12 <2 6 N/A N/A N/A N/A <2 >12 <2 <2 6 N/A N/A N/A N/A <2 >12 <2 <2 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) PB-SI(180),FE-SI(180),BA- SI(180),AG-SI(180),AS- SI(180),CU-SI(180),MN- SI(180),NA-SI(180),CD- SI(180),CR-SI(180),CA- SI(180),HG-S(28),SE- SI(180),ZN-SI(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) CU-6020S(180),FE-SI(180),BA- SI(180),AS-SI(180),MN- SI(180),NA-SI(180),PB- 6020S(180),AG-6020S(180),CR- SI(180),CA-SI(180),CD- 6020S(180),HG-S(28),SE- SI(180),ZN-SI(180) HARDT(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) CU-6020S(180),FE-SI(180),BA- SI(180),AS-SI(180),MN- SI(180),NA-SI(180),PB- 6020S(180),AG-6020S(180),CR- SI(180),CA-SI(180),CD- 6020S(180),HG-S(28),SE- SI(180),ZN-SI(180) HARDT(180) Project Name: Project Number: L1304045Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/18/13 Serial_No:03181313:41 Page 78 of 87 *Values in parentheses indicate holding time in days L1304045-08I L1304045-09A L1304045-09B L1304045-09C L1304045-09D L1304045-09E L1304045-09F L1304045-09G L1304045-09H L1304045-09I L1304045-10A Plastic 500ml unpreserved Vial HCl preserved Vial HCl preserved Vial HCl preserved Plastic 250ml unpreserved Plastic 250ml H2SO4 preserved Plastic 250ml NaOH preserved Plastic 250ml HNO3 preserved Plastic 250ml HNO3 preserved Plastic 500ml unpreserved Vial HCl preserved A A A A A A A A A A A 6 N/A N/A N/A N/A <2 >12 <2 <2 6 N/A 4 4 4 4 4 4 4 4 4 4 4 Y Y Y Y Y Y Y Y Y Y Y Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent Absent NANTUCKET LF 1910-97168-CG.SAMP CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) 8260(14) 8260(14) ALK-T-2320(14) COD-5220(28) TCN-9010(14) CU-6020S(180),FE-SI(180),BA- SI(180),AS-SI(180),MN- SI(180),NA-SI(180),PB- 6020S(180),AG-6020S(180),CR- SI(180),CA-SI(180),CD- 6020S(180),HG-S(28),SE- SI(180),ZN-SI(180) HARDT(180) CL-9251(28),SO4- 9038(28),NO3-4500(2),TDS- 2540(7) 8260(14) Project Name: Project Number: L1304045Lab Number: Report Date: Container ID Container Type Cooler pH Temp deg C Pres Seal Container Information Analysis(*) 03/18/13 Serial_No:03181313:41 Page 79 of 87 Report Format:Data Usability Report GLOSSARY Project Name: Project Number: Lab Number: Report Date: L1304045NANTUCKET LF 1910-97168-CG.SAMP 03/18/13 Acronyms EDL EPA LCS LCSD LFB MDL MS MSD NA NC NI RL RPD SRM Estimated Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The EDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. The use of EDLs is specific to the analysis of PAHs using Solid-Phase Microextraction (SPME). Environmental Protection Agency. Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Laboratory Control Sample Duplicate: Refer to LCS. Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes. Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS. Not Applicable. Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit. Not Ignitable. Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable. Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precision of analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report. Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples. - - - - - - - - - - - - - - Terms Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum. Data Qualifiers A B C D E G H I - - - - - - - - Spectra identified as "Aldol Condensation Product". The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ- Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit. Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses. Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte. Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument. The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated. The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection. The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reported 1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the original method. - Footnotes Serial_No:03181313:41 Page 80 of 87 Report Format:Data Usability Report Project Name: Project Number: Lab Number: Report Date: L1304045NANTUCKET LF 1910-97168-CG.SAMP 03/18/13 Data Qualifiers M NJ P Q R RE - - - - - - due to obvious interference. Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte. Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search. The RPD between the results for the two columns exceeds the method-specified criteria. The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing Calibration Standard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoveries when the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are less than 5x the RL. (Metals only.) Analytical results are from sample re-analysis. Analytical results are from sample re-extraction. J ND - - Estimated value. This represents an estimated concentration for Tentatively Identified Compounds (TICs). Not detected at the reporting limit (RL) for the sample. Serial_No:03181313:41 Page 81 of 87 Alpha Analytical performs services with reasonable care and diligence normal to the analytical testing laboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analytical shall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liable for any incidental, consequential or special damages, including but not limited to, damages in any way connected with the use of, interpretation of, information or analysis provided by Alpha Analytical. We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling, containers, sampling procedures, holding time and splitting of samples in the field. LIMITATION OF LIABILITIES 1 30 Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997. Standard Methods for the Examination of Water and Wastewater. APHA-AWWA- WPCF. 18th Edition. 1992. Project Name: Project Number: Lab Number: Report Date: L1304045NANTUCKET LF 1910-97168-CG.SAMP REFERENCES 03/18/13 Serial_No:03181313:41 Page 82 of 87 Certificate/Approval Program Summary Last revised December 19, 2012 - Westboro Facility The following list includes only those analytes/methods for which certification/approval is currently held. For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative. Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4- Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O- Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl- D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 6010C, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223B, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8330, 8151A, 8260B, 8260C, 8270C, 8270D, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014, 9030B, 9040B, 9045C, 6010B, 6010C, 6020, 6020A, 7471A, 7471B, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8270D, 8330, 8151A, 8081A, 8081B, 8082, 8082A, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2- Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Serial_No:03181313:41 Page 83 of 87 Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7 for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW- 846 6010C, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9010C, 9030, 9040B, 9040C, SM2120B, 2310B, 2320B, 2340B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 4500SO3-B, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082A, 8081B, 8015C, 8151A, 8330, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010C, 6020A, 7196A, 7471B, 1010, 1010A, 1030, 9010C, 9012B, 9014, 9030B, 9040C, 9045C, 9045D, 9050, 9065, 9251, 1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3620D, 3630C, 5030B, 5035, 8260C, 8270D, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 9040C, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010C, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8011, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9030B, 1010, 1010A, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9010C, 9012B, 9014, 9038, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3620C, 3630C, 5030B, 5035L, 5035H, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 7470A, SM2120B, LACHAT 10-204- 00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010C, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012B, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010C, 9030B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C, Serial_No:03181313:41 Page 84 of 87 3546, 3580A, 5030B, 5035A-H, 5035A-L.) North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7470A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F- C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 350.1, 350.2, 351.1, 353.2, 420.1, 6010C, 6020A, 7196A, 7470A, 9030B, 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NH3-H, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C, 9010C, 9040C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D-SIM, 8330, 8015C, NJ-EPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010C, 6020A, 7196A, 7471B, 9010C, 9012B, 9014, 9040B, 9045D, 9050A, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3620C, 3630C, 5035, 8015C, 8081B, 8082A, 8151A, 8260C, 8270D, 8270D- SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL- E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 200.8, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5030B, 5035, 3540C, 3546, 355B0, 3580A, 3630C, 6020A, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056, 7196A, 3500-Cr-D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.) Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C, Serial_No:03181313:41 Page 85 of 87 8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease. Serial_No:03181313:41 Page 86 of 87 Serial_No:03181313:41 Page 87 of 87 Appendix D Landfill Gas Notification to MassDEP